Ethyl 2-amino-7,7-dimethyl-2′,5-dioxospiro[5,6,7,8-tetrahydro-4H-chromene-4,3′(2′H)-1H-indole]-3-carboxylate

被引:1
作者
Wang, Jing [1 ]
Zhu, Song-Lei [1 ]
机构
[1] Xuzhou Med Coll, Dept Chem, Xuzhou 221004, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
Data-to-parameter ratio = 13.1; Mean σ(C-C) = 0.003 Å; R factor = 0.049; Single-crystal X-ray study; T = 153 K; WR factor = 0.107;
D O I
10.1107/S1600536809055809
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the molecule of the title compound, C21H22N2O5, the indole system and the spiro-pyran ring are almost planar [maximum deviations of 0.0447 (17) and 0.0781 (17) angstrom, respectively]; the dihedral angle between them is 84.6 (3)degrees. The remaining six-membered ring adopts a twisted conformation. Intramolecular N-H center dot center dot center dot O hydrogen bonds occur. In the crystal structure, interamolecular N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds link the molecules.
引用
收藏
页码:O302 / U1899
页数:11
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