1H and 13C spectral assignment of naphtho[2′,1′:5,6]naphtho[2′,1′:4,5]thieno[2,3-c]quinoline using the IDR-GHSQC-TOCSY experiment

被引：5

作者：

Hadden, CE

Martin, GE ^{[1
]}

Luo, JK

Castle, RN

机构：

[1] Pharmacia Corp, Pharmaceut Dev, Rapid Struct Characterizat Grp, Kalamazoo, MI 49001 USA

[2] Univ S Florida, Dept Chem, Tampa, FL 33620 USA

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2000年 / 37卷 / 04期

关键词：

D O I：

10.1002/jhet.5570370425

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The assignment of the NMR spectra of the polynuclear heteroaromatic naphtho[2',1':5,6]naphtho-[2',1':4,5]thieno[2,3-c]quinoline is reported. The analysis was based on the homonuclear ROESY, heteronuclear direct GHSQC, IDR-GHSQC-TOCSY, and long-range GHMBC experiments. The complete H-1 and C-13 Shift assignments are reported.

引用

页码：821 / 825

页数：5

共 13 条

[1] SENSITIVITY-ENHANCED TWO-DIMENSIONAL HETERONUCLEAR SHIFT CORRELATION NMR-SPECTROSCOPY [J].

BAX, A ;

SUBRAMANIAN, S .

JOURNAL OF MAGNETIC RESONANCE, 1986, 67 (03) :565-569

[2] COMPARISON OF DIFFERENT MODES OF 2-DIMENSIONAL REVERSE-CORRELATION NMR FOR THE STUDY OF PROTEINS [J].

BAX, A ;

IKURA, M ;

KAY, LE ;

TORCHIA, DA ;

TSCHUDIN, R .

JOURNAL OF MAGNETIC RESONANCE, 1990, 86 (02) :304-318

[3] NATURAL ABUNDANCE N-15 NMR BY ENHANCED HETERONUCLEAR SPECTROSCOPY [J].

BODENHAUSEN, G ;

RUBEN, DJ .

CHEMICAL PHYSICS LETTERS, 1980, 69 (01) :185-189

[4] PURE ABSORPTION PHASE GRADIENT-ENHANCED HMQC-TOCSY WITH DIRECT RESPONSE EDITING [J].

CROUCH, RC ;

DAVIS, AO ;

MARTIN, GE .

MAGNETIC RESONANCE IN CHEMISTRY, 1995, 33 (11) :889-892

[5] A NEW METHOD TO DISTINGUISH BETWEEN DIRECT AND REMOTE SIGNALS IN PROTON-RELAYED X,H CORRELATIONS [J].

DOMKE, T .

JOURNAL OF MAGNETIC RESONANCE, 1991, 95 (01) :174-177

[6] A comparison of the hyphenated experiments GHMQC-TOCSY and GHSQC-TOCSY [J].

Hadden, CE ;

Martin, GE ;

Luo, JK ;

Castle, RN .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1999, 36 (02) :533-539

[7] GRADIENT-ENHANCED PROTON-DETECTED HETERONUCLEAR MULTIPLE-QUANTUM COHERENCE SPECTROSCOPY [J].

HURD, RE ;

JOHN, BK .

JOURNAL OF MAGNETIC RESONANCE, 1991, 91 (03) :648-653

[8] INVERTED AND SUPPRESSED DIRECT RESPONSE HMQC-TOCSY SPECTRA - A CONVENIENT METHOD OF SPECTRAL EDITING [J].

MARTIN, GE ;

SPITZER, TD ;

CROUCH, RC ;

LUO, JK ;

CASTLE, RN .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1992, 29 (02) :577-582

[9]

Parella T, 1998, MAGN RESON CHEM, V36, P467, DOI 10.1002/(SICI)1097-458X(199807)36:7<467::AID-OMR325>3.0.CO

[10]

2-S

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