An exploratory investigation on the in-situ synthesis of SiC/AlN/Al composites by spark plasma sintering

被引:30
作者
Daoush, W. [2 ]
Francis, A. [1 ]
Lin, Y. [3 ]
German, R. [3 ]
机构
[1] Cent Met Res & Dev Inst, Cairo, Egypt
[2] Helwan Univ, Fac Ind Educ, Prod Technol Dept, Cairo, Egypt
[3] San Diego State Univ, Coll Engn, Dept Mech Engn, San Diego, CA 92182 USA
关键词
Spark plasma sintering (SPS); Al/SiCN composites; Hardness; Microstructure; MECHANICAL-PROPERTIES; MATRIX COMPOSITES; CERAMICS; ALUMINUM; NANOCOMPOSITES; CONSOLIDATION; CONDUCTIVITY; EXTRUSION; BEHAVIOR; SYSTEM;
D O I
10.1016/j.jallcom.2014.10.066
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The powder mixtures of aluminum and silicon carbonitride (Al-SiCN) have been consolidated into bulk materials by spark plasma sintering. XRD patterns indicated the in-situ formation of SiC and AlN. The density of the SiCN-Al composite sintered by SPS at 500 degrees C is 2.65 g/cm(3) or higher in a weight range of SiCN powder particles up to 2.5%. The formation of new phases and the relatively absence of porosities in the matrix composites are attributed to the co-existence of solid-liquid state that leads to the effective densification of the mixed powders. The breakdown of SiCN network structure was considered to result from a reaction between partially aluminum melt and SiCN particles. An improvement in density and hardness is observed. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:458 / 462
页数:5
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