Synthesis of Co3O4 nanorod bunches from a single precursor CO(CO3)0.35Cl0.20(OH)1.10

被引：59
|
作者：
Wang, ZH
Chen, XY
Zhang, M
Qian, YT [1 ]
机构：
[1] Univ Sci & Technol China, Struct Res Lab, Anhua 230026, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China
来源：
SOLID STATE SCIENCES | 2005年 / 7卷 / 01期
基金：
中国国家自然科学基金;
关键词：
nanorod bunches; thermal decomposition; CO3O4; precursor;
D O I：
10.1016/j.solidstatesciences.2004.10.032
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
CO3O4 nanorods were successfully synthesized from a single precursor via a thermal decomposition and oxidization route. The precursor used was Co(CO3)(0.35)Cl-0.20(OH)(1.10), which was prepared by a hydrothermal reaction using CoCl2(.)6H(2)O with CO(NH2)(2) at 95-120degreesC. Both the precursor and the as-prepared Co3O4 were characterized with XRD, TEM, SEM, TGA and XPS. The precursor, as well as CO3O4, was found to be composed of nanorods that were radially bunched. The Co3O4 nanorods obtained through a thermal treatment at 300 degreesC for 5 h were found to have a porous structure. (C) 2004 Elsevier SAS. All rights reserved.
引用
收藏
页码：13 / 15
页数：3
相关论文
共 50 条
  • [31] Nanocrystalline Co3O4 fabricated via the combustion method
    Makhlouf, M. Th.
    Abu-Zied, B. M.
    Mansoure, T. H.
    METALS AND MATERIALS INTERNATIONAL, 2013, 19 (03) : 489 - 495
  • [32] CoO and Co3O4 nanoparticles with a tunable particle size
    Bartunek, Vilem
    Huber, Stepan
    Sedmidubsky, David
    Sofer, Zdenek
    Simek, Petr
    Jankovsky, Ondfej
    CERAMICS INTERNATIONAL, 2014, 40 (08) : 12591 - 12595
  • [33] Synthesis and characterization of Co3O4 nanoplates by simple thermolysis of the [Co(NH3)6]2(C2O4)3•4H2O complex
    Farhadi, Saeed
    Pourzare, Kolsoum
    Sadeghinejad, Shokooh
    POLYHEDRON, 2014, 67 : 104 - 110
  • [34] Solvothermal synthesis of morphology controllable CoCO3 and their conversion to Co3O4 for catalytic application
    Jing, Xiaoyan
    Song, Shanshan
    Wang, Jun
    Ge, Lan
    Jamil, Saba
    Liu, Qi
    Mann, Tom
    He, Yang
    Zhang, Milin
    Wei, Hao
    Liu, Lianhe
    POWDER TECHNOLOGY, 2012, 217 : 624 - 628
  • [35] Characterization of atomic layer deposited semiconducting Co3O4
    Holden, Konner E. K.
    Conley, John F., Jr.
    JOURNAL OF VACUUM SCIENCE & TECHNOLOGY A, 2019, 37 (02):
  • [36] Low temperature solvothermal synthesis of pristine Co3O4 nanoparticles as potential supercapacitor
    UmaSudharshini, A.
    Bououdina, M.
    Venkateshwarlu, M.
    Manoharan, C.
    Dhamodharan, P.
    SURFACES AND INTERFACES, 2020, 19
  • [37] Rapid synthesis of nanocrystalline Co3O4 by a microwave-assisted combustion method
    Ai, Lun-Hong
    Jiang, J.
    POWDER TECHNOLOGY, 2009, 195 (01) : 11 - 14
  • [38] Green synthesis of Co3O4 nanoparticles via Aspalathus linearis: Physical properties
    Diallo, A.
    Beye, A. C.
    Doyle, T. B.
    Park, E.
    Maaza, M.
    GREEN CHEMISTRY LETTERS AND REVIEWS, 2015, 8 (3-4) : 30 - 36
  • [39] Synthesis and calcinations effects on size analysis of Co3O4 nanospheres and their superparamagnetic behaviors
    Babu, G. Anandha
    Ravi, G.
    Hayakawa, Y.
    Kumaresavanji, M.
    JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2015, 375 : 184 - 193
  • [40] Facile synthesis of bimodal mesoporous spinel Co3O4 nanomaterials and their structural properties
    Pudukudy, Manoj
    Yaakob, Zahira
    Narayanan, Binitha
    Gopalakrishnan, Anila
    Tasirin, Siti Masrinda
    SUPERLATTICES AND MICROSTRUCTURES, 2013, 64 : 15 - 26
12345