3,3′-Ethylenebis(3,4-dihydro-6-chloro-2H-1,3-benzoxazine)

被引：5

作者：

Rivera, Augusto ^{[1
]}

Jose Rojas, Jicli ^{[1
]}

Rios-Motta, Jaime ^{[1
]}

Dusek, Michal ^{[2
]}

Fejfarova, Karla ^{[2
]}

机构：

[1] Univ Nacl Colombia, Dept Quim, Bogota 14490, Colombia

[2] Inst Phys, Prague 18221 8, Czech Republic

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

D O I：

10.1107/S1600536810014248

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The asymmetric unit of the title compound, C(18)H(18)Cl(2)N(2)O(2), contains one half of an independent molecule, the other half being generated via a centre of inversion at the molecular centroid. In the crystal structure, molecular chains are formed through non-classical C-H center dot center dot center dot O hydrogen bonds between an axial H atom of the oxazine ring and the O atom of a neighbouring molecule.

引用

页码：O1134 / U620

页数：9

共 13 条

[1]

[Anonymous], 2009, CRYSALIS CCD CRYSALI

[2] IMIDAZOLIDINES .3. 2-SUBSTITUTED 1,3-BIS-(O-HYDROXYBENZYL)-IMIDAZOLIDINES [J].

BILLMAN, JH ;

DORMAN, LC .

JOURNAL OF MEDICINAL CHEMISTRY, 1963, 6 (06) :701-&

[3]

Brandenburg K., 2005, DIAMOND

[4]

Burla M. C., 2003, Journal of Applied Crystallography, V36, DOI 10.1107/S0021889803012585

[5] 3-benzyl-6-methyl-3,4-dihydro-2H-1,3-benzoxazine [J].

Chen, Xiu-Ling ;

Wu, Ming-Hu .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :O3684-U1925

[6] THE ANALYTICAL CALCULATION OF ABSORPTION IN MULTIFACETED CRYSTALS [J].

CLARK, RC ;

REID, JS .

ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :887-897

[7] Highly antibacterial active aminoacyl penicillin conjugates with acylated bis-catecholate siderophores based on secondary diamino acids and related compounds [J].

Heinisch, L ;

Wittmann, S ;

Stoiber, T ;

Berg, A ;

Ankel-Fuchs, D ;

Möllmann, U .

JOURNAL OF MEDICINAL CHEMISTRY, 2002, 45 (14) :3032-3040

[8] 1,4-Bis(8-tert-butyl-6-methyl-4H-1,3-benzoxazin-3-yl)benzene [J].

Huerta, Raul ;

Toscano, Ruben A. ;

Castillo, Ivan .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O2938-O2940

[9]

Petricek V., 2006, JANA2006

[10] 3,3′-(p-Phenylene)bis(3,4-dihydro-2H-1,3-benzoxazine) [J].

Ranjith, Sekaran ;

Thenmozhi, Sundar ;

Manikannan, Ramaiyan ;

Muthusubramanian, Shanmugam ;

Subbiahpandi, Arunachalathevar .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O581-U2333

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