4-Methoxybenzaldehyde (phthalazin-1-ylidene)hydrazone

被引：12
作者：
Butcher, Ray J.
Jasinski, Jerry P.
Yathirajan, H. S.
Vijesh, A. M.
Narayana, B.
机构：
[1] Keene State Coll, Dept Chem, Keene, NH 03435 USA
[2] Howard Univ, Dept Chem, Washington, DC 20059 USA
[3] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India
[4] Mangalore Univ, Dept Studies Chem, Mangalagangothri 574199, India
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷
关键词：
ANTIMICROBIAL ACTIVITY; SCHIFF; DERIVATIVES; BASES;
D O I：
10.1107/S1600536807037051
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C16H14N4O, crystallizes with two independent molecules in the asymmetric unit. The phthalazin-1-yl and 4-methoxybenzaldehyde groups are coplanar with each other in each of the independent molecules with angles between their mean planes of 15.4 ( 4) and 13.3 (9)degrees. The crystal packing is stabilized by intermolecular N-H center dot center dot center dot N hydrogen bonding between inverted phthalazin-1-yl groups allowing the independent molecules to be stacked in groups oblique to the ab plane in a zigzag pattern.
引用
收藏
页码：O3674 / U1830
页数：12
相关论文
共 12 条
[1]  
Aydogan F, 2001, B KOR CHEM SOC, V22, P476
[2]  
Desai SB, 2001, HETEROCYCL COMMUN, V7, P83
[3]   Synthesis and antimicrobial activity of some new benzimidazole derivatives [J].
El-masry, AH ;
Fahmy, HH ;
Abdelwahed, SHA .
MOLECULES, 2000, 5 (12) :1429-1438
[4]  
Farrugia L. J. J., 1999, Appl. Crystallogr, V32, P837, DOI [10.1107/S0021889812029111, DOI 10.1107/S0021889812029111]
[5]   STRUCTURE-ANTITUMOR ACTIVITY CORRELATION OF SOME SCHIFF BASES [J].
HODNETT, EM ;
DUNN, WJ .
JOURNAL OF MEDICINAL CHEMISTRY, 1970, 13 (04) :768-&
[6]   1-(2-Pyridyl)ethan-1-one 8-quinolylhydrazone and 1-(1H-pyrrol-2-yl)ethan-1-one 8-quinolylhydrazone [J].
Lynch, DE ;
McClenaghan, I .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2002, 58 :o642-o644
[7]   4-Methyl-2-(8-quinolyl)phthalazin-1-one [J].
Lynch, DE ;
McClenaghan, I .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 :O1051-O1052
[8]  
*OXF DIFF LTD, 2007, CRYSALISPRO VERS 171
[9]   Synthesis and antimicrobial activity of Schiff and Mannich bases of isatin and its derivatives with pyrimidine [J].
Pandeya, SN ;
Sriram, D ;
Nath, G ;
De Clercq, E .
FARMACO, 1999, 54 (09) :624-628
[10]  
Sheldrick G.M., 1997, SHELXS-97, a Program for the Automatic Solution of Crystal Structures
12