Solid-phase synthesis of traceless 1,3-diketones

被引：9

作者：

Park, KH ^{[1
]}

Cox, LJ ^{[1
]}

机构：

[1] DuPont Co Inc, Cent Res & Dev, Expt Stn, Wilmington, DE 19880 USA

来源：

TETRAHEDRON LETTERS | 2003年 / 44卷 / 05期

关键词：

D O I：

10.1016/S0040-4039(02)02720-X

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A traceless synthesis of 1,3-diketones has been achieved through enamine methodology from solid-phase organic synthesis. Thus, piperazine served as a linker for this traceless cleavage of D-diketones from solid support. (C) 2003 Elsevier Science Ltd. All rights reserved.

引用

页码：1067 / 1069

页数：3

共 19 条

[1] Alekseev V.V., 1995, RUSS J ORG CHEM+, V31, P868
[2] ELLIOT JM, 2002, 223 ACS NAT M APR 7
[3] TITANIUM-INDUCED SYNTHESES OF FURANS AND INDOLES
FURSTNER, A
JUMBAM, DN
WEIDMANN, H
[J]. TETRAHEDRON LETTERS, 1991, 32 (46) : 6695 - 6696
[4] Some aspects of competitive coordination of β-diketones and nitrogen-containing ligands
Garnovskii, AD
Kharisov, BI
Blanco, LM
Garnovskii, DA
Burlov, AS
Vasilchenko, IS
Bondarenko, GI
[J]. JOURNAL OF COORDINATION CHEMISTRY, 1999, 46 (04) : 365 - 395
[5] HAUSER CR, 1954, ORG REACTIONS, V8, P59
[6] ENAMINES - RECENT ADVANCES IN SYNTHETIC, SPECTROSCOPIC, MECHANISTIC, AND STEREOCHEMICAL ASPECTS .1.
HICKMOTT, PW
[J]. TETRAHEDRON, 1982, 38 (14) : 1975 - 2050
[7] Solid phase synthesis of 2-aminobutadienes using a piperazine linker
Hird, NW
Irie, K
Nagai, K
[J]. TETRAHEDRON LETTERS, 1997, 38 (40) : 7111 - 7114
[8] Synthesis of β-dicarbonyl compounds using 1-acylbenzotriazoles as regioselective C-acylating reagents
Katritzky, AR
Pastor, A
[J]. JOURNAL OF ORGANIC CHEMISTRY, 2000, 65 (12) : 3679 - 3682
[9] VARIETY IN THE COORDINATION MODES OF BETA-DICARBONYL COMPOUNDS IN METAL-COMPLEXES
KAWAGUCHI, S
[J]. COORDINATION CHEMISTRY REVIEWS, 1986, 70 : 51 - 84
[10] RECENT DEVELOPMENTS IN ISOXAZOLE CHEMISTRY
KOCHETKOV, NK
SOKOLOV, SD
[J]. ADVANCES IN HETEROCYCLIC CHEMISTRY, 1963, 2 : 365 - 422

← 1 2 →