Pressurized liquid extraction: A useful technique to extract pharmaceuticals and personal-care products from sewage sludge

被引:133
作者
Nieto, Antonio [1 ]
Borrull, Francesc [1 ]
Pocurull, Eva [1 ]
Maria Marce, Rosa [1 ]
机构
[1] Univ Rovira & Virgili, Dept Analyt Chem & Organ Chem, Tarragona 43007, Spain
关键词
Contaminant; Extraction; Personal-care product; Pharmaceutical; PPCP; Pressurized liquid extraction; Sample preparation; Sewage sludge; Solvent; Volatile organic; TANDEM MASS-SPECTROMETRY; WASTE-WATER TREATMENT; SOLID-PHASE EXTRACTION; GAS CHROMATOGRAPHY/MASS SPECTROMETRY; ACCELERATED SOLVENT-EXTRACTION; ENVIRONMENTAL-SAMPLES; POLYCHLORINATED-BIPHENYLS; POLYCYCLIC MUSKS; TREATMENT PLANTS; UV FILTERS;
D O I
10.1016/j.trac.2010.03.014
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
We review the determination of pharmaceuticals and personal-care products (PPCPs) in sewage-sludge samples using pressurized liquid extraction (PLE). PLE is a sample-preparation technique that is increasingly used to extract moderately volatile and non-volatile organic contaminants from solid samples. We discuss the principal parameters to be optimized in PLE (e.g., solvent extraction, temperature, pressure and extraction time). We also examine the occurrence of PPCPs in studies where PLE is applied to sewage sludge. (C) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码:752 / 764
页数:13
相关论文
共 54 条
[1]   Multi-residue determination of pharmaceuticals in sludge and sludge enriched soils using pressurized liquid extraction, solid phase extraction and liquid chromatography with tandem mass spectrometry [J].
Barron, Leon ;
Tobin, John ;
Paull, Brett .
JOURNAL OF ENVIRONMENTAL MONITORING, 2008, 10 (03) :353-361
[2]   Pressurized fluid extraction of polychlorinated biphenyls in solid environmental samples [J].
Björklund, E ;
Bowadt, S ;
Nilsson, T ;
Mathiasson, L .
JOURNAL OF CHROMATOGRAPHY A, 1999, 836 (02) :285-293
[3]   Novel analytical procedures for screening of drug residues in water, waste water, sediment and sludge [J].
Buchberger, Wolfgang W. .
ANALYTICA CHIMICA ACTA, 2007, 593 (02) :129-139
[4]  
Büyüksönmez F, 2005, J RESIDUALS SCI TECH, V2, P31
[5]   Simultaneous determination of triclocarban and triclosan in municipal biosolids by liquid chromatography tandem mass spectrometry [J].
Chu, Shaogang ;
Metcalfe, Cms D. .
JOURNAL OF CHROMATOGRAPHY A, 2007, 1164 (1-2) :212-218
[6]   Some aspects of the analysis of environmental pollutants in sediments using pressurized liquid extraction and gas chromatography-mass spectrometry [J].
Dabrowski, L ;
Giergielewicz-Mozajska, H ;
Biziuk, M ;
Gaca, J ;
Nameisnik, J .
JOURNAL OF CHROMATOGRAPHY A, 2002, 957 (01) :59-67
[7]   Analysis of selected emerging contaminants in sewage sludge [J].
Diaz-Cruz, M. S. ;
Garcia-Galan, M. J. ;
Guerra, P. ;
Jelic, A. ;
Postigo, C. ;
Eljarrat, E. ;
Farre, M. ;
de Alda, M. J. Lopez ;
Petrovic, M. ;
Barcelo, D. .
TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2009, 28 (11) :1263-1275
[8]   Determination of antimicrobials in sludge from infiltration basins at two artificial recharge plants by pressurized liquid extraction-liquid chromatography-tandem mass spectrometry [J].
Diaz-Cruz, M. Silvia ;
Lopez de Alda, M. Jose ;
Barcelo, Damia .
JOURNAL OF CHROMATOGRAPHY A, 2006, 1130 (01) :72-82
[9]   Application of pressurized liquid extraction followed by gas chromatography-mass spectrometry to determine 4-nonylphenols in sediments [J].
Ding, WH ;
Fann, JCH .
JOURNAL OF CHROMATOGRAPHY A, 2000, 866 (01) :79-85
[10]   Improved liquid chromatographic determination of nine currently used (fluoro)quinolones with fluorescence and mass spectrometric detection for environmental samples [J].
Ferdig, M ;
Kaleta, A ;
Buchberger, W .
JOURNAL OF SEPARATION SCIENCE, 2005, 28 (13) :1448-1456