Microwave-assisted hydrothermal synthesis and characterization of CeO2 nanowires for using as a photocatalytic material

被引:49
作者
Phuruangrat, Anukorn [1 ]
Thongtem, Somchai [2 ,3 ]
Thongtem, Titipun [4 ]
机构
[1] Prince Songkla Univ, Fac Sci, Dept Mat Sci & Technol, Hat Yai 90112, Songkhla, Thailand
[2] Chiang Mai Univ, Fac Sci, Dept Phys & Mat Sci, Chiang Mai 50200, Thailand
[3] Chiang Mai Univ, Fac Sci, Mat Sci Res Ctr, Chiang Mai 50200, Thailand
[4] Chiang Mai Univ, Fac Sci, Dept Chem, Chiang Mai 50200, Thailand
关键词
Microwave-assisted hydrothermal synthesis; CeO2; nanowires; Photocatalysis; FLOW SYNTHESIS; NANO-RODS; NANOPARTICLES; ARRAYS;
D O I
10.1016/j.matlet.2017.03.013
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
One-dimensional CeO2 materials were successfully synthesized by a microwave assisted hypothermal method at 100, 120 and 140 degrees C for 30 min. Phase and morphology of the products were investigated by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Their XRD patterns were specified as pure CeO2 cubic phase. Their TEM images presented uniform CeO2 nanorods for the synthesis temperatures of 100 degrees C and 120 degrees C and nanowires with high aspect ratio and their growth along the [110] direction for the synthesis temperature of 140 degrees C. The photocatalytic activities of CeO2 samples were investigated through degradation of methyl orange (MO) as a representative dye pollutant under UV light irradiation. The CeO2 nanowires have the highest photodegradation of 98% within 100 min. (C) 2017 Elsevier B. V. All rights reserved.
引用
收藏
页码:61 / 63
页数:3
相关论文
共 20 条
[1]   Continuous microwave flow synthesis and characterization of nanosized tin oxide [J].
Akram, Muhammad ;
Alshemary, Ammar Z. ;
Butt, Faheem K. ;
Goh, Yi-Fan ;
Ibrahim, Wan Aini Wan ;
Hussain, Rafaqat .
MATERIALS LETTERS, 2015, 160 :146-149
[2]   Continuous microwave flow synthesis (CMFS) of nanosized titania: Structural, optical and photocatalytic properties [J].
Akram, Muhammad ;
Butt, Faheem K. ;
Alshemary, Ammar Z. ;
Goh, Yi-Fan ;
Ibrahim, Wan Aini Wan ;
Hussain, Rafaqat .
MATERIALS LETTERS, 2015, 158 :95-98
[3]   Microwave-assisted synthesis of functional electrode materials for energy applications [J].
Butt, Faheem K. ;
Bandarenka, Aliaksandr S. .
JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2016, 20 (11) :2915-2928
[4]   Synthesis and characterization of CeO2 nano-rods [J].
Chen, Yong ;
Liu, Tianmo ;
Chen, Chunlin ;
Guo, Weiwei ;
Sun, Rong ;
Lv, Shuhui ;
Saito, Mitsuhiro ;
Tsukimoto, Susumu ;
Wang, Zhongchang .
CERAMICS INTERNATIONAL, 2013, 39 (06) :6607-6610
[5]   Hydrothermal synthesis of ceria hybrid architectures of nano-rods and nano-octahedrons [J].
Chen, Yong ;
Liu, Tianmo ;
Chen, Chunlin ;
Guo, Weiwei ;
Sun, Rong ;
Lv, Shuhui ;
Saito, Mitsuhiro ;
Tsukimoto, Susumu ;
Wang, Zhongchang .
MATERIALS LETTERS, 2013, 96 :210-213
[6]   A controllable microwave-assisted hydrothermal method to synthesize ZnO nanowire arrays as recyclable photocatalyst [J].
Ge, Xing ;
Hong, Kunquan ;
Zhang, Jiao ;
Liu, Liqing ;
Xu, Mingxiang .
MATERIALS LETTERS, 2015, 139 :119-121
[7]   Controllable synthesis, characterization, and CO oxidation activity of CeO2 nanostructures with various morphologies [J].
He, Haiyan ;
Yang, Ping ;
Li, Jia ;
Shi, Ruixia ;
Chen, Ling ;
Zhang, Aiyu ;
Zhu, Yuanna .
CERAMICS INTERNATIONAL, 2016, 42 (06) :7810-7818
[8]   One-step method for growing of large scale ZnO nanowires on zinc foil [J].
Ji, Yajun .
MATERIALS LETTERS, 2015, 138 :92-95
[9]   Fabrication of micropillar TiO2 photocatalyst arrays using nanoparticle-microprinting method [J].
Kameya, Yuki ;
Yamaki, Hiroshi ;
Ono, Reiya ;
Motosuke, Masahiro .
MATERIALS LETTERS, 2016, 175 :262-265
[10]   Exploration of CeO2 nanoparticles as a chemi-sensor and photo-catalyst for environmental applications [J].
Khan, Sher Bahadar ;
Faisal, M. ;
Rahman, Mohammed M. ;
Jamal, Aslam .
SCIENCE OF THE TOTAL ENVIRONMENT, 2011, 409 (15) :2987-2992