SYNTHESIS AND CRYSTAL STRUCTURE OF β-N-(5-METHYL-4-OXO-5,6-DIHYDRO-4H-1,3-THIAZIN-2-YL)ISONICOTINOHYDRAZIDE

被引：6

作者：

Kulakov, I. V. ^{[1
]}

Turdybekov, D. M. ^{[2
]}

Nurkenov, O. A. ^{[1
]}

Issabaeva, G. M. ^{[1
]}

Makhmutova, A. S. ^{[2
]}

Turdybekov, K. M. ^{[2
]}

Fazylov, S. D. ^{[1
]}

机构：

[1] Inst Organ Synth & Coal Chem Kazakhstan Republ, Karaganda 100008, Kazakhstan

[2] Minist Educ & Sci Republ Kazakhstan, Res & Prod Ctr Phytochem, Karaganda 100009, Kazakhstan

来源：

CHEMISTRY OF HETEROCYCLIC COMPOUNDS | 2009年 / 45卷 / 09期

关键词：

methacryloylthiosemicarbazide of isonicotinic acid; intramolecular heterocyclization; X-ray crystallography;

D O I：

10.1007/s10593-009-0398-0

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

In the presence of amines under mild conditions, beta-N-(methacryloylcarbamoythioyl) isonicotinohydrazide underwent intramolecular heterocyclization to give alpha-N-(5-methyl-4-oxo-5,6-dihydro4H-1,3-thiazin-2-yl) isonicotinohydrazide, the spatial structure was confirmed by X-ray crystallography.

引用

页码：1117 / 1120

页数：4

共 4 条

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[2]

Burla M. C., 2003, Journal of Applied Crystallography, V36, DOI 10.1107/S0021889803012585

[3] SYNTHESIS AND HETEROCYCLIZATION OF β-N-(METHACRYLOYLTHIOCARBAMOYL)-ISONICOTINOHYDRAZIDE [J].

Kulakov, I. V. .

CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2008, 44 (07) :889-890

[4]

SHELDRICK GM, SHELXL 97 CRYSTAL ST

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