A Simple and Quick Chemical Synthesis of Nanostructured Bi2Te3, Sb2Te3, and BixSb2-xTe3

被引：7
|
作者：
Kim, HeeJin [1 ]
Lee, Ki Jung [2 ]
Kim, Sung-Jin [1 ]
Han, Mi-Kyung [1 ]
机构：
[1] Ewha Womans Univ, Dept Chem & Nano Sci, Seoul 120750, South Korea
[2] Northfield Mt Hermon Sch 12th, Mt Hermon, MA USA
来源：
BULLETIN OF THE KOREAN CHEMICAL SOCIETY | 2010年 / 31卷 / 05期
关键词：
Bi2Te3; Sb2Te3; BixSb2-xTe3; Nanoparticle; Thermoelectric material; BISMUTH TELLURIDE NANOPARTICLES; MICROWAVE-ASSISTED SYNTHESIS; DEVICES; ALLOYS; ROUTE; MERIT;
D O I：
10.5012/bkcs.2010.31.5.1123
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We report a simple and quick route for the preparation of high-quality, nearly monodisperse Bi2Te3, Sb2Te3, and BixSb2-xTe3 nanocrystallites. The reactions of bismuth acetate or antimony acetate with Te in oleic acid result in pure phase of Bi2Te3 or Sb2Te3 nanoparticles, respectively. Also, ternary BixSb2-xTe3 nanoparticles were successfully synthesized using the same method. The size and morphology of the nanoparticles were controlled by varying the stabilizing agents. The as-prepared nanoparticles are characterized by X-ray diffraction, scanning electron microscope, and high-resolution transmission electron microscope using an energy dispersive spectroscopy.
引用
收藏
页码：1123 / 1127
页数：5
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