Photometric determination of tetracycline based on surface plasmon resonance of silver nanoparticles

被引：16

作者：

Amjadi, Mohammad ^{[1
]}

Manzoori, Jamshid L. ^{[1
]}

Pakpoor, Faezeh ^{[1
]}

机构：

[1] Univ Tabriz, Dept Analyt Chem, Fac Chem, Tabriz 5166616471, Iran

来源：

JOURNAL OF ANALYTICAL CHEMISTRY | 2016年 / 71卷 / 03期

关键词：

tetracycline; silver nanoparticles; surface plasmon resonance; LIQUID-CHROMATOGRAPHIC METHOD; LIGHT-SCATTERING; CHEMILUMINESCENCE DETERMINATION; FLUORESCENCE DETECTION; RESIDUES; ANTIBIOTICS; MILK; HPLC; OXYTETRACYCLINE; VALIDATION;

D O I：

10.1134/S1061934816030072

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

We report on a simple and sensitive method for the determination of tetracycline based on its reducing action on AgNO3 in alkaline medium containing ammonia and sodium hydroxide at 65A degrees C. As a result of this reaction, silver nanoparticles (AgNPs) are formed. The AgNPs are stabilized in solution by adding poly(vinyl pyrrolidone) as a capping agent. The formed AgNPs were identified by surface plasmon resonance absorption spectrum and transmission electron microscopy image. The plasmon absorption peak at 411 nm is proportional to the concentration of tetracycline. The calibration graph is linear in the concentration range of 0.05-5.0 mg/L with a detection limit of 0.013 mg/L. This method was applied to the determination of tetracycline in pharmaceutical products.

引用

页码：253 / 258

页数：6

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