N-benzoyl-N′-(3-hydroxyphenyl)thiourea

被引：6

作者：

Abosadiya, Hamza Milad ^{[1
]}

Yamin, Bohari M. ^{[1
]}

Ngah, Nurziana ^{[1
]}

机构：

[1] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Selangor 43600, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷

关键词：

D O I：

10.1107/S1600536807016509

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C14H12N2O2S, the benzoyl and 3-hydroxyphenyl fragments adopt trans-cis positions with respect to the S atom across their C-N bonds. The dihedral angle between the 3-hydroxyphenyl and N2CS thiourea groups is 72.09 ( 8) degrees. The crystal structure is stabilized by O-H center dot center dot center dot S and N-H center dot center dot center dot S hydrogen bonds, forming a polymeric chain along the c axis.

引用

页码：O2403 / O2404

页数：2

共 7 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2]

*BRUK AXS INC, 2000, SADABS VERS 2 01 SMA

[3]

Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI DOI 10.1107/S0021889895007138

[4]

Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR, P38

[5]

SHELDRICK GM, 1997, SHELXTL VERSION 5 10

[6] Single-crystal structure validation with the program PLATON [J].

Spek, AL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13

[7] N′-benzoyl-N-p-bromophenylthiourea [J].

Yamin, BM ;

Yusof, MSM .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 :O340-O341

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