Synthesis and characterization of Bi2S3 nanorods by solvothermal method in polyol media

被引：27
|
作者：
Zhang, Hong
Wang, Lijiu
机构：
[1] Dalian Univ Technol, Sch Civil & Hydraul Engn, Dalian 116024, Peoples R China
[2] Dalian Inst Light Ind, Sch Chem Ind & Mat, Dalian 116034, Peoples R China
来源：
MATERIALS LETTERS | 2007年 / 61卷 / 8-9期
关键词：
D O I：
10.1016/j.matlet.2006.07.095
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Bi2S3 nanorods were synthesized via a simple solvothermal process in polyol media through the reaction between Bi(NO3)(3)center dot 5H(2)O, urea and CS2 at 150 degrees C for 15 h using diethylene glycol as solvent. The nanorods were characterized by XRD, TEM and SAED. The results showed that the products were well-crystallized orthorhombic phase with lattice parameters a=11.15 angstrom, b=11.3 angstrom and c=3.984 angstrom, which are consistent with the value in standard JCPDS card No. 17-0320. DEG served as an excellent solvent and structure director. Besides, compared to water and EG as solvents, the DEG system can provide a mild and homogenous condition, which is favorable to anisotropic growth and increases the yield of high quality Bi2S3 nanorods. Based on the experimental results, the growth mechanism was discussed. (c) 2006 Elsevier B.V. All rights reserved.
引用
收藏
页码：1667 / 1670
页数：4
相关论文
共 50 条
  • [1] Bi2S3 nanoflowers and nanorods synthesized by solvothermal method
    Yuan, AH
    Wang, P
    Pang, L
    Zhou, H
    Ma, H
    CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2006, 22 (03) : 559 - 562
  • [2] Surfactant-assisted solvothermal synthesis of Bi2S3 nanorods
    Ma, Xiao-Yong
    Liu, Lu
    Mo, Wen-Ling
    Liu, Huajie
    Kou, Hui-Zhong
    Wang, Yuqiu
    JOURNAL OF CRYSTAL GROWTH, 2007, 306 (01) : 159 - 165
  • [3] Solvothermal synthesis and characterization of ultralong Bi2S3 nanowires
    Ye, Mingfu
    Sun, Qingjiang
    Lu, Yafei
    Yi, Tingfeng
    Chen, Guochang
    Xu, Lixin
    Journal of Advanced Microscopy Research, 2014, 9 (01) : 58 - 61
  • [4] Polyol-mediated preparation of Bi2S3 nanorods
    Wang, DB
    Shao, MW
    Yu, DB
    Li, GP
    Qian, YT
    JOURNAL OF CRYSTAL GROWTH, 2002, 243 (02) : 331 - 335
  • [5] Synthesis and characterization of Bi/Bi2S3 nanocomposite through polyol method and its photovoltaic applications
    Zeynali, Hossein
    Mousavi, Seyed Behnam
    Hosseinpour-Mashkani, S. Mostafa
    MATERIALS LETTERS, 2015, 144 : 65 - 68
  • [6] Preparation of CdS nanowires and Bi2S3 nanorods by extraction-solvothermal method
    Shi, HQ
    Zhou, XD
    Fu, X
    Wang, DB
    Hu, ZS
    MATERIALS LETTERS, 2006, 60 (15) : 1793 - 1795
  • [7] Solvothermal synthesis of Bi2S3 nanoparticles and nanorods towards solar cell application
    Arumugam, J.
    Raj, A. Dhayal
    Irudayaraj, A. Albert
    Thambidurai, M.
    MATERIALS LETTERS, 2018, 220 : 28 - 31
  • [8] Synthesis, Characterization and Optical Property of Uniform Bi2S3 Nanorods
    Liu, Shuling
    Shi, Qiangqiang
    Tong, Jianbo
    Li, Shu
    Li, Miaomiao
    CHINESE CERAMICS COMMUNICATIONS II, 2012, 412 : 211 - 214
  • [9] Facile solvothermal synthesis of single-crystalline Bi2S3 nanorods on a large scale
    Yang, XH
    Wang, X
    Zhang, ZD
    MATERIALS CHEMISTRY AND PHYSICS, 2006, 95 (01) : 154 - 157
  • [10] Characterization of Bi2S3 nanorods prepared at room temperature
    Deshpande, M. P.
    Sakariya, Pallavi N.
    Bhatt, Sandip V.
    Garg, Nitya
    Patel, Kamakshi
    Chaki, S. H.
    MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING, 2014, 21 : 180 - 185
12345