Biomolecule-assisted Solvothermal Synthesis of Bismuth Sulfide Nanorods

被引：21

作者：

Zhong, Jiasong ^{[1
]}

Xiang, Weidong ^{[1
,2
]}

Liu, Lijun ^{[1
]}

Yang, Xinyu ^{[1
]}

Cai, Wen ^{[2
]}

Zhang, Jingfeng ^{[1
]}

Liang, Xiaojuan ^{[1
]}

机构：

[1] Wenzhou Univ, Coll Chem & Mat Engn, Wenzhou 325035, Peoples R China

[2] Tongji Univ, Coll Mat Sci & Engn, Shanghai 200092, Peoples R China

来源：

JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY | 2010年 / 26卷 / 05期

关键词：

Bismuth sulfide; Solvothermal; L-cystine; Nanorods; ELECTROCHEMICAL HYDROGEN STORAGE; HYDROTHERMAL SYNTHESIS; BI2S3; NANORODS; OPTICAL-PROPERTIES; NANOWIRES; GROWTH; CYSTEINE; NANOSTRUCTURES; PBS; ARCHITECTURES;

D O I：

10.1016/S1005-0302(10)60065-5

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A simple biomolecule-assisted synthetic route has been successfully developed to prepare bismuth sulfide (Bi2S3) nanorods under solvothermal conditions. In the synthetic system, pentahydrate bismuth nitrate was employed to supply Bi source and L-cystine was used as sulfide source and complexing agent. The morphology, structure, and phase composition of the as-prepared Bi2S3 products were characterized by X-ray diffraction (XRD), energy dispersion spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and high-resolution transmission electron microscopy (HRTEM). The experimental results show that the nanorods have uniform diameter of 100-200 nm and length of 2-4 mu m. The possible formation mechanism for the bismuth sulfide nanorods was discussed.

引用

页码：417 / 422

页数：6