The use of DTA/TGA to study the effects of ground quartz with different surface areas in autoclaved cement:quartz pastes.: Use of the semi-isothermal thermogravimetric technique

被引:24
作者
Klimesch, DS
Ray, A
机构
[1] Univ Technol Sydney, Dept Mat Sci, Sydney, NSW 2007, Australia
[2] James Hardie & Coy Pty Ltd, Sydney, NSW 2142, Australia
关键词
autoclaving; carbonation; cement : quartz; semi-isothermal thermogravimetry; quartz fineness;
D O I
10.1016/S0040-6031(97)00279-7
中图分类号
O414.1 [热力学];
学科分类号
摘要
Simultaneous DTA-TG and derivative thermogravimetry, DTG, have been employed to evaluate autoclaved cement : quartz pastes, before and after carbonation. DTG curves provided more detailed information about mass loss phenomena than the corresponding TG curves. Results indicated that the dynamic method did not allow sufficient time for reactions to be completed. Data obtained from dynamic methods can be used to carry out semi-isothermal thermogravimetry very successfully, the latter allowing separation of peaks due to overlapping decomposition phenomena. (C) 1997 Published by Elsevier Science B.V.
引用
收藏
页码:159 / 165
页数:7
相关论文
共 22 条
[1]  
BAKER LR, 1980, INT J CONCRETE MASON, V2, P75
[2]  
BAOZHEN S, 1984, GUISUANYAN SUEBAO, V12, P281
[3]   DETERMINATION OF FREE LIME AND CARBONATE IN CALCIUM SILICATE HYDRATES BY THERMOBALANCE [J].
BIFFEN, FM .
ANALYTICAL CHEMISTRY, 1956, 28 (07) :1133-1136
[4]  
BUTT YM, 1973, 3 INT S AUT BUILD MA
[5]  
COLE WF, 1959, NATURE, V184, P57
[6]  
DANIELS T, 1973, THERM ANAL, P56
[7]  
EBERT R, 1978, INT S BEZ ZWISCH EIG, V17
[8]   SIMULTANEOUS SEMI-ISOTHERMAL METHOD OF THERMOGRAVIMETRY AND DERIVATIVE THERMOGRAVIMETRY, AND ITS APPLICATION TO CEMENT PASTES [J].
ELJAZAIRI, B ;
ILLSTON, JM .
CEMENT AND CONCRETE RESEARCH, 1977, 7 (03) :247-258
[9]  
Gaze R., 1956, MAG CONCRETE RES, V8, P7, DOI [10.1680/macr.1956.8.22.7, DOI 10.1680/MACR.1956.8.22.7]
[10]   CALCIUM SILICATE CARBONATION PRODUCTS [J].
GOTO, S ;
SUENAGA, K ;
KADO, T ;
FUKUHARA, M .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1995, 78 (11) :2867-2872