Sucrose solution as a new viscous test fluid with tunable viscosities up to 2 Pas for micromixing characterization by the Villermaux-Dushman reaction

被引:6
|
作者
Arian, Elias [1 ]
Pauer, Werner [1 ]
机构
[1] Univ Hamburg, Dept Tech & Macromol Chem, Bundesstr 45, D-20146 Hamburg, Germany
关键词
Villermaux-dushman reaction; Micromixing; Viscous medium; Iodide-iodate method; High viscosity; COMPETING REACTION SYSTEM; MIXING EFFICIENCY; TIME; FLOW;
D O I
10.1007/s41981-021-00158-1
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
For the first time, micromixing characterization for the Villermaux-Dushman reaction could be performed with a non-reactive viscous medium at viscosities up to 2 Pas. As viscous medium, sucrose solution was used with the benefit of being a Newtonian fluid with tuneable viscosity. Due to the higher viscosities in comparison to established media for micromixing investigations, a new protocol for the experimental implementation was developed. Micromixing experiments were conducted and the applicability of viscous sucrose solutions was proven in a stirred tank reactor. Major challenges in characterizing micromixing efficiency in high viscous solution were consolidated.
引用
收藏
页码:579 / 588
页数:10
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