A novel precursor in preparation and characterization of nickel oxide nanoparticles via thermal decomposition approach

被引：145

作者：

Salavati-Niasari, Masoud ^{[1
,2
]}

Mir, Noshin ^{[2
]}

Davar, Fatemeh ^{[1
]}

机构：

[1] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran

[2] Univ Kashan, Fac Chem, Dept Inorgan Chem, Kashan, Iran

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2010年 / 493卷 / 1-2期

关键词：

Nanostructured materials; Chemical synthesis; P-TYPE NIO; ZNO NANOPARTICLES; BETA-NI(OH)(2); NANOCRYSTALS; FABRICATION; MORPHOLOGY; COMPLEX; FILM;

D O I：

10.1016/j.jallcom.2009.11.153

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

In order to raise the need of co-surfactant in the synthesis of NiO nanoparticles, [bis(2-hydroxy-1-naphthaldehydato)nickel(II)] complex was employed as a novel precursor in thermal decomposition process using oleylamine (C18H37N) as surfactant. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA), X-ray photoelectron spectroscopy (XPS) and ultraviolet-visible (UV-Vis) spectroscopy. Also the novel precursor thermally was treated in solid state reaction in different temperature, 400, 500, and 600 degrees C. Synthesized nickel oxide nanoparticles have a cubic phase with average size of 15-20 nm. (C) 2009 Elsevier B.V. All rights reserved.

引用

页码：163 / 168

页数：6

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