Redetermination of 1,3,5-trichloro-2,4-dinitrobenzene

被引：3

作者：

Kruger, PE ^{[1
]}

Mackie, PR

Nieuwenhuyzen, M

机构：

[1] Univ Dublin Trinity Coll, Dept Chem, Dublin 2, Ireland

[2] Queens Univ Belfast, Sch Chem, Belfast BT9 5AG, Antrim, North Ireland

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 2000年 / 56卷

关键词：

D O I：

10.1107/S0108270100013998

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title compound, C6HCl3N2O4, is an intermediate in the synthesis of 1,3,5-trichloro-2,4,6-trinitrobenzene. The crystal structure at 153 K shows no major deviations from the previously reported structure at 295 K other than the expected contraction of the a and c axes and, correspondingly, the beta angle.

引用

页码：E532 / E532

页数：1

共 10 条

[1]

*BRUK AXS INC, 1999, SMART SAINT VERS 6 0

[2]

*BRUK AXS INC, 1998, SHELXTL VERS 5 10

[3] Identification of organic compounds I Chlorosuffonic acid as a reagent for the identification of aryl halides [J].

Huntress, EH ;

Carten, FH .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1940, 62 :511-514

[4]

JACKSON CL, 1887, AM CHEM J, V9, P348

[5] REDUCTION OF NITROAROMATIC COMPOUNDS WITH SODIUM BOROHYDRIDE [J].

KAPLAN, LA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1964, 86 (04) :740-&

[6]

KOHNE B, 1985, LIEBIGS ANN CHEM, P522

[7] ELECTROPHILIC AROMATIC-SUBSTITUTION .32. THE NITRATION OF 1,3,5-TRICHLORO-2-NITROBENZENE, "1,3,5-TRICHLORO-2,6-DINITROBENZENE, AND 1,2,3,5-TETRACHLORO-4,6-DINITROBENZENE IN SULFURIC-ACID AND IN OLEUM [J].

MOODIE, RB ;

PAYNE, MA ;

SCHOFIELD, K .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1985, (09) :1457-1464

[8]

PRAEFCKE K, 1989, LIEBIGS ANN CHEM, P617

[9]

RODGERS DZ, 1986, J ORG CHEM, V51, P3904

[10] CL-35 NQR SPECTRA AND CRYSTAL-STRUCTURES OF 1,2,4,5-TETRACHLORO-3,6-DINITROBENZENE AND OF 1,3,5-TRICHLORO-2,4-DINITROBENZENE [J].

WIGAND, S ;

WALZ, L ;

WEIDEN, N ;

WEISS, A .

BERICHTE DER BUNSEN-GESELLSCHAFT-PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 1987, 91 (11) :1189-1194

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