A green synthesis of isatoic anhydrides from isatins with urea-hydrogen peroxide complex and ultrasound

被引:26
作者
Deligeorgiev, Todor [1 ]
Vasilev, Aleksey
Vaquero, Juan J.
Alvarez-Builla, Julio
机构
[1] Univ Sofia, Fac Chem, Sofia 1164, Bulgaria
[2] Univ Alcala de Henares, Fac Pharm, Alcala De Henares 28871, Madrid, Spain
关键词
D O I
10.1016/j.ultsonch.2006.12.003
中图分类号
O42 [声学];
学科分类号
070206 ; 082403 ;
摘要
The oxidation of isatins at room temperature, using the cheap and environmentally friendly urea-hydrogen peroxide complex and ultrasonic irradiation, has been investigated. The ultrasonic irradiation dramatically reduces the reaction time. With easy and reproducible reaction procedures, different isatoic anhydrides were obtained in excellent yield and with high purity. (c) 2006 Elsevier B.V. All rights reserved.
引用
收藏
页码:497 / 501
页数:5
相关论文
共 44 条
[31]  
1971, Patent No. 1950281
[32]  
1980, Patent No. 4177041
[33]  
1982, Patent No. 3045911
[34]  
1974, Patent No. 2218328
[35]  
1980, Patent No. 54135739
[36]  
1939, Patent No. 2150968
[37]  
1982, Patent No. 4313873
[38]  
1913, Patent No. 259826
[39]  
1988, Patent No. 3602014
[40]  
1979, Patent No. 54018970