New experimental set-ups for studying nanoconfined water on the AILES beamline at SOLEIL

被引：22

作者：

Bernardina, S. Dalla ^{[1
]}

Alabarse, F. ^{[1
]}

Kalinko, A. ^{[1
]}

Roy, P. ^{[1
]}

Chapuis, M. ^{[1
]}

Vita, N. ^{[1
]}

Hienerwadel, R. ^{[2
]}

Berthomieu, C. ^{[3
]}

Judeinstein, P. ^{[4
]}

Zanotti, J. -M. ^{[4
]}

Bantignies, J. L. ^{[6
]}

Haines, J. ^{[5
]}

Catafesta, J. ^{[5
]}

Creff, G. ^{[7
]}

Manceron, L. ^{[1
]}

Brubach, J. -B. ^{[1
]}

机构：

[1] LOrme Merisiers, Soc Civile Synchrotron SOLEIL, F-91192 Gif Sur Yvette, France

[2] Aix Marseille Univ, Lab Genet & Biophys Plantes, F-13108 St Paul Les Durance, France

[3] IBEB, DSV, CEA, Lab Interact Proteine Met, F-13108 St Paul Les Durance, France

[4] CNRS, CEA, Lab Leon Brillouin, UMR12, F-91191 Gif Sur Yvette, France

[5] Univ Montpellier 2, CNRS, Inst Charles Gerhardt, UMR 5253, F-34095 Montpellier 5, France

[6] Univ Montpellier 2, CNRS UM2, Dept CVN, Lab Charles Coulomb,UMR 5221, F-34095 Montpellier 5, France

[7] Univ Nice Sophia Antipolis, Inst Chim Nice, F-06108 Nice, France

来源：

VIBRATIONAL SPECTROSCOPY | 2014年 / 75卷

关键词：

Synchrotron radiation; FTIR; Infrared absorption spectroscopy; Difference spectroscopy; Water; Vibrations; Hydrogen bond; Adsorbates on surfaces; Vycor; Molecules; Framework; Faujasite; Metalloprotein; FAR-INFRARED SPECTROSCOPY; SYNCHROTRON-RADIATION; LIGHT-SOURCE; X-RAY; DIFFERENCE SPECTROSCOPY; TEMPERATURE-DEPENDENCE; PRESSURE; AMORPHIZATION; DIFFRACTION; TRANSITION;

D O I：

10.1016/j.vibspec.2014.07.016

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Three ensembles designed to investigate condensed matter in complex environments have been developed recently on the AILES beamline at SOLEIL. They have been exploited for studies aiming at understanding the properties of water molecules and their network in various confining systems, namely: - a hydration and temperature-controlled cell for the study of water confined in nanoporous Vycor, - a high pressure set-up allowing the study of the evolution of water molecules network trapped in Faujasite through the pressure-induced amorphisation of the matrix material, - a temperature resolved electrochemical cell used to record FIR difference spectra of metalloproteins interacting with water molecules. By combining the high infrared flux and collimation of the AILES beamline with these optimized sample environments, it is possible to measure the infrared and THz spectra for minute quantities of samples in precise physical conditions. (C) 2014 Elsevier B.V. All rights reserved.

引用

页码：154 / 161

页数：8

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