Separation of gallic acid from Cornus officinalis Sieb. et Zucc by high-speed counter-current chromatography

被引：46
|
作者：
Tian, GL [1 ]
Zhang, TY
Yang, FQ
Ito, Y
机构：
[1] Beijing Inst New Technol Applicat, Beijing 100035, Peoples R China
[2] NHLBI, Biophys Chem Lab, NIH, Bethesda, MD 20892 USA
来源：
JOURNAL OF CHROMATOGRAPHY A | 2000年 / 886卷 / 1-2期
关键词：
Cornus officinalis; counter-current chromatography; gallic acid;
D O I：
10.1016/S0021-9673(00)00480-5
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Gallic acid was separated from a n-butanol extract of the fruit of Cornus officinalis Sieb. et Zucc by high-speed countercurrent chromatography in two steps using two solvent systems composed of ethyl-acetate-ethanol n-butanol-water (5:1.8:6, v/v/v) and ethyl acetate-ethanol-water (5:0.5:6, v/v/v) successively. From 1 g of n-butanol extract the method produced 60 mg of gallic acid at a purity of 97%. (C) 2000 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：309 / 312
页数：4
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