Preparation and Characterization of Nano-Sized Magnetic Particles LaCoO3 by Ultrasonic-Assisted Coprecipitation Method

被引:36
作者
Khorasani-Motlagh, Mozhgan [1 ]
Noroozifar, Meissam [1 ]
Jahani, Shohreh [1 ]
机构
[1] Univ Sistan & Baluchestan, Dept Chem, Zahedan, Iran
关键词
LaCoO3; perovskite oxide; ultrasonic; coprecipitation; nanocrystals; PEROVSKITE; NANOPARTICLES; DISPERSION; OXIDES;
D O I
10.1080/15533174.2015.1031010
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A study on the synthesis of LaCoO3 nanocrystals using a new ultrasonic process has been carried out by comparing the formation time with the same factor under conventional coprecipitation process. The samples are characterized by Fourier transform infrared spectroscopy (FTIR), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray (EDX). Magnetic measurements are carried out by a vibrating sample magnetometer (VSM) on the product at room temperature. While both powder exhibited the same XRD patterns indexed as pure perovskite structure, their homogeneity is found to be strongly influenced by the preparation method.
引用
收藏
页码:1591 / 1595
页数:5
相关论文
共 16 条
[1]   Preparation of ZnS nanorods by ultrasonic waves [J].
Behboudnia, M ;
Majlesara, MH ;
Khanbabaee, B .
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2005, 122 (02) :160-163
[2]   Oxide solid solutions as catalysts [J].
Cimino, A ;
Stone, FS .
ADVANCES IN CATALYSIS, VOL 47, 2002, 47 :141-306
[3]   THE TEMPERATURE OF CAVITATION [J].
FLINT, EB ;
SUSLICK, KS .
SCIENCE, 1991, 253 (5026) :1397-1399
[4]   Preparation and gas-sensitive properties of LaFe1-yCoyO3 semiconducting materials [J].
Ge, XT ;
Liu, YF ;
Liu, XQ .
SENSORS AND ACTUATORS B-CHEMICAL, 2001, 79 (2-3) :171-174
[5]   Synthesis of superparamagnetic Mn3O4 nanocrystallites by ultrasonic irradiation [J].
Gopalakrishnan, IK ;
Bagkar, N ;
Ganguly, R ;
Kulshreshtha, SK .
JOURNAL OF CRYSTAL GROWTH, 2005, 280 (3-4) :436-441
[6]   Pure phase LaFeO3 perovskite with improved surface area synthesized using different routes and its characterization [J].
Gosavi, Priti V. ;
Biniwale, Rajesh B. .
MATERIALS CHEMISTRY AND PHYSICS, 2010, 119 (1-2) :324-329
[7]   Reducibility of Co3+ in perovskite-type LaCoO3 and promotion of copper on the reduction of Co3+ in perovskite-type oxides [J].
Huang, L ;
Bassir, M ;
Kaliaguine, S .
APPLIED SURFACE SCIENCE, 2005, 243 (1-4) :360-375
[8]   HIGH IONIC-CONDUCTIVITY IN LITHIUM LANTHANUM TITANATE [J].
INAGUMA, Y ;
CHEN, LQ ;
ITOH, M ;
NAKAMURA, T ;
UCHIDA, T ;
IKUTA, H ;
WAKIHARA, M .
SOLID STATE COMMUNICATIONS, 1993, 86 (10) :689-693
[9]   Dispersion control of Fe2O3 nanoparticles using a mixed type of mechanical and ultrasonic milling [J].
Lee, CS ;
Lee, JS ;
Oh, ST .
MATERIALS LETTERS, 2003, 57 (18) :2643-2646
[10]   FTIR spectral characterization of thin film coatings of oleic acid on glasses: I. Coatings on glasses from ethyl alcohol [J].
Lee, DH ;
Condrate, RA .
JOURNAL OF MATERIALS SCIENCE, 1999, 34 (01) :139-146