High-throughput powder diffraction measurement system consisting of multiple MYTHEN detectors at beamline BL02B2 of SPring-8

被引：270
作者：
Kawaguchi, S. [1 ]
Takemoto, M. [1 ]
Osaka, K. [2 ]
Nishibori, E. [3 ,4 ]
Moriyoshi, C. [5 ]
Kubota, Y. [6 ]
Kuroiwa, Y. [5 ]
Sugimoto, K. [1 ]
机构：
[1] Japan Synchrotron Radiat Res Inst JASRI, Res & Utilizat Div, SPring 8,1-1-1 Kouto, Sayo, Hyogo 6795198, Japan
[2] Japan Synchrotron Radiat Res Inst JASRI, Ind Applicat Div, SPring 8,1-1-1 Kouto, Sayo, Hyogo 6795198, Japan
[3] Univ Tsukuba, TIMS, Fac Pure & Appl Sci, Tsukuba, Ibaraki 3058571, Japan
[4] Univ Tsukuba, CiRfSE, Tsukuba, Ibaraki 3058571, Japan
[5] Hiroshima Univ, Grad Sch Sci, Higashihiroshima, Hiroshima 7398526, Japan
[6] Osaka Prefecture Univ, Dept Phys Sci, Sakai, Osaka 5998531, Japan
来源：
REVIEW OF SCIENTIFIC INSTRUMENTS | 2017年 / 88卷 / 08期
关键词：
SWISS LIGHT-SOURCE; METAL-INSULATOR TRANSITIONS; DEBYE-SCHERRER CAMERA; MATERIALS SCIENCE; DIFFRACTOMETER;
D O I：
10.1063/1.4999454
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
In this study, we developed a user-friendly automatic powder diffraction measurement system for Debye-Scherrer geometry using a capillary sample at beamline BL02B2 of SPring-8. The measurement system consists of six one-dimensional solid-state (MYTHEN) detectors, a compact autosampler, wide-range temperature control systems, and a gas handling system. This system enables to do the automatic measurement of temperature dependence of the diffraction patterns for multiple samples. We introduced two measurement modes in the MYTHEN system and developed new attachments for the sample environment such as a gas handling system. The measurement modes and the attachments can offer in situ and/or time-resolved measurements in an extended temperature range between 25 K and 1473 K and various gas atmospheres and pressures. The results of the commissioning and performance measurements using reference materials (NIST CeO2 674b and Si 640c), V2O3 and Ti2O3, and a nanoporous coordination polymer are presented. Published by AIP Publishing.
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页数：9
相关论文
共 30 条
[1]  
[Anonymous], 1987, GEN STRUCTURE ANAL S
[2]   Photon counting microstrip detector for time resolved powder diffraction experiments [J].
Bergamaschi, A. ;
Cervellino, A. ;
Dinapoli, R. ;
Gozzo, F. ;
Henrich, B. ;
Johnson, I. ;
Kraft, P. ;
Mozzanica, A. ;
Schmitt, B. ;
Shi, X. .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2009, 604 (1-2) :136-139
[3]   The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source [J].
Bergamaschi, Anna ;
Cervellino, Antonio ;
Dinapoli, Roberto ;
Gozzo, Fabia ;
Henrich, Beat ;
Johnson, Ian ;
Kraft, Philipp ;
Mozzanica, Aldo ;
Schmitt, Bernd ;
Shi, Xintian .
JOURNAL OF SYNCHROTRON RADIATION, 2010, 17 :653-668
[4]   The high resolution powder diffraction beam line at ESRF [J].
Fitch, AN .
JOURNAL OF RESEARCH OF THE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY, 2004, 109 (01) :133-142
[5]   Electric field induced lattice strain in pseudocubic Bi(Mg1/2Ti1/2)O3-modified BaTiO3-BiFeO3 piezoelectric ceramics [J].
Fujii, Ichiro ;
Iizuka, Ryo ;
Nakahira, Yuki ;
Sunada, Yuya ;
Ueno, Shintaro ;
Nakashima, Kouichi ;
Magome, Eisuke ;
Moriyoshi, Chikako ;
Kuroiwa, Yoshihiro ;
Wada, Satoshi .
APPLIED PHYSICS LETTERS, 2016, 108 (17)
[6]   First experiments at the Swiss Light Source Materials Science beamline powder diffractometer [J].
Gozzo, F ;
Schmitt, B ;
Bortolamedi, T ;
Giannini, C ;
Guagliardi, A ;
Lange, M ;
Meister, D ;
Maden, D ;
Willmott, P ;
Patterson, BD .
JOURNAL OF ALLOYS AND COMPOUNDS, 2004, 362 (1-2) :206-217
[7]   X-ray pair distribution function analysis of nanostructured materials using a Mythen detector [J].
Haverkamp, Richard G. ;
Wallwork, Kia S. .
JOURNAL OF SYNCHROTRON RADIATION, 2009, 16 :849-856
[8]   A Series of Layered Assemblies of Hydrogen-Bonded, Hexagonal Networks of C3-Symmetric π-Conjugated Molecules: A Potential Motif of Porous Organic Materials [J].
Hisaki, Ichiro ;
Nakagawa, Shoichi ;
Ikenaka, Nobuaki ;
Imamura, Yutaka ;
Katouda, Michio ;
Tashiro, Motomichi ;
Tsuchida, Hiromu ;
Ogoshi, Tomoki ;
Sato, Hiroyasu ;
Tohnai, Norimitsu ;
Miyata, Mikiji .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2016, 138 (20) :6617-6628
[9]   Metal-insulator transitions [J].
Imada, M ;
Fujimori, A ;
Tokura, Y .
REVIEWS OF MODERN PHYSICS, 1998, 70 (04) :1039-1263
[10]   Note: An X-ray powder diffractometer with a wide scattering-angle range of 72° using asymmetrically positioned one-dimensional detectors [J].
Katsuya, Yoshio ;
Song, Chulho ;
Tanaka, Masahiko ;
Ito, Kimihiko ;
Kubo, Yoshimi ;
Sakata, Osami .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2016, 87 (01)
123