Isolation and structure determination of a lignan from the bark of Salix alba

被引:15
作者
Du, Qizhen [1 ]
Jerz, Gerold
Shen, Lianqing
Xiu, Lili
Winterhalter, Peter
机构
[1] Zhejiang Gongshang Univ, Res Ctr Bioact Food, Hangzhou 310035, Peoples R China
[2] Tech Univ Braunschweig, Inst Food Chem, DE-38106 Braunschweig, Germany
关键词
lignan; sisymbrifolin; Salix alba; ESI-MS; 2D-NMR;
D O I
10.1080/14786410601083845
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A lignan, sisymbrifolin ( 1) found in the fruits of Solanum sisymbriflolium has been isolated from the bark extract of Salix alba ( Salicaceae). Its structure was elucidated by its direct spectrum data of ESI-MS and one- and two-dimensional NMR spectroscopy for the first time.
引用
收藏
页码:451 / 454
页数:4
相关论文
共 14 条
[1]   MALDI-TOF mass spectrometry and PSD fragmentation as means for the analysis of condensed tannins in plant leaves and needles [J].
Behrens, A ;
Maie, N ;
Knicker, H ;
Kögel-Knabner, I .
PHYTOCHEMISTRY, 2003, 62 (07) :1159-1170
[2]   A neolignan and sterols in fruits of Solanum sisymbrifolium [J].
Chakravarty, AK ;
Mukhopadhyay, S ;
Saha, S ;
Pakrashi, SC .
PHYTOCHEMISTRY, 1996, 41 (03) :935-939
[3]   Treatment of low back pain with a herbal or synthetic anti-rheumatic:: a randomized controlled study.: Willow bark extract for low back pain [J].
Chrubasik, S ;
Künzel, O ;
Model, A ;
Conradt, C ;
Black, A .
RHEUMATOLOGY, 2001, 40 (12) :1388-1393
[4]   Treatment of low back pain exacerbations with willow bark extract: A randomized double-blind study [J].
Chrubasik, S ;
Eisenberg, E ;
Balan, E ;
Weinberger, T ;
Luzzati, R ;
Conradt, C .
AMERICAN JOURNAL OF MEDICINE, 2000, 109 (01) :9-14
[5]   Semi-industrial isolation of salicin and amygdalin from plant extracts using slow rotary counter-current chromatography [J].
Du, QZ ;
Jerz, G ;
He, YC ;
Li, L ;
Xu, YJ ;
Zhang, Q ;
Zheng, QX ;
Winterhalter, P ;
Ito, Y .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1074 (1-2) :43-46
[6]   Preparation of three flavonoids from the bark of Salix alba by high-speed countercurrent chromatographic separation [J].
Du, QZ ;
Jerz, G ;
Winterhalter, P .
JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, 2004, 27 (20) :3257-3264
[7]  
Fiebich BL, 2004, PHYTOMEDICINE, V11, P135, DOI 10.1016/j.phymed.2004.03.003
[8]  
KARACSONYI S, 1983, CELL CHEM TECHNOL, V17, P637
[9]   FLAVONOIDS FROM SALIX-ALBA-STRUCTURE OF TERNIFLORIN AND ANOTHER ACYLFLAVONOID [J].
KARL, C ;
MULLER, G ;
PEDERSEN, PA .
PHYTOCHEMISTRY, 1976, 15 (06) :1084-1085
[10]  
KOMPANTSEV VA, 1976, CHEM NATURAL COMPOUN