Effect of Methane Pressure on the Size of Carbon Nanoparticles Deposited by Pulsed Plasma Enhanced Chemical Vapor Deposition

被引:0
作者
Rastkar, Ahmad R. [1 ]
Shokri, Babak [1 ]
Kabir, Mojtaba [1 ]
Amirzadeh, Maria [2 ]
Rahimipour, Mohammad R. [3 ]
机构
[1] Shahid Beheshti Univ, Laser & Plasma Res Inst, Plasma Engn Grp, GC, Tehran, Iran
[2] Shahid Beheshti Univ, Sch Earth Sci, GC, Tehran, Iran
[3] Mat & Energy Res Ctr, Karaj, Iran
关键词
carbon; CVD; methane; nanoparticles; plasma pulsed dc; AMORPHOUS-CARBON; DIAMOND; BLACK; RAMAN;
D O I
10.1002/ppap.200932207
中图分类号
O59 [应用物理学];
学科分类号
摘要
The nanoparticles of carbon were deposited from methane under the potential of a pulsed direct current discharge. The deposition was carried without external heating. The size, chemistry, and structure of carbon nanoparticles were characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), Raman and Fourier transform infrared (FTIR) spectroscopy. The minimum size of the nanoparticles was as low as 10 nm as shown by TEM. The nanocrystalline or amorphous structure of the particles was revealed by XRD. Raman spectroscopy indicated on the sp(2) bonds of carbon and FTIR spectroscopy identified the other bonds of carbon.
引用
收藏
页码:S855 / S859
页数:5
相关论文
共 20 条
[1]  
[Anonymous], 1975, Introduction to infrared and Raman spectroscopy
[2]   Collection and characterization of airborne nanoparticulates [J].
Bang, JJ ;
Murr, LE ;
Esquivel, EV .
MATERIALS CHARACTERIZATION, 2004, 52 (01) :1-14
[3]  
BOLOURI KS, 1983, J B SOC CHIM FR, V5, pL101
[4]   One-step catalyst-free generation of carbon nanospheres via laser-induced pyrolysis of anthracene [J].
Bystrzejewski, M. ;
Lange, H. ;
Huczko, A. ;
Baranowski, P. ;
Huebers, H.-W. ;
Gemming, T. ;
Pichler, T. ;
Buechner, B. ;
Ruemmeli, M. H. .
JOURNAL OF SOLID STATE CHEMISTRY, 2008, 181 (10) :2796-2803
[5]   TRIBOLOGICAL AND ELECTRICAL-PROPERTIES OF METAL-CONTAINING HYDROGENATED CARBON-FILMS [J].
DIMIGEN, H ;
HUBSCH, H ;
MEMMING, R .
APPLIED PHYSICS LETTERS, 1987, 50 (16) :1056-1058
[6]  
Donnet J.B., 1993, CARBON BLACK, V2nd
[7]   STUDY OF TRANSFORMATION OF DIAMOND TO GRAPHITE [J].
EVANS, T ;
JAMES, PF .
PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1964, 277 (1368) :260-+
[8]   Carbon black processing by thermal plasma. Analysis of the particle formation mechanism [J].
Fabry, F ;
Flamant, G ;
Fulcheri, L .
CHEMICAL ENGINEERING SCIENCE, 2001, 56 (06) :2123-2132
[9]   XPS and laser Raman analysis of hydrogenated amorphous carbon films [J].
Filik, J ;
May, PW ;
Pearce, SRJ ;
Wild, RK ;
Hallam, KR .
DIAMOND AND RELATED MATERIALS, 2003, 12 (3-7) :974-978
[10]   Experimental study of fullerene-family formation using radio-frequency-discharge reactive plasmas [J].
Ishida, H ;
Satake, N ;
Jeong, GH ;
Abe, Y ;
Hirata, T ;
Hatakeyama, R ;
Tohji, K ;
Motomiya, K .
THIN SOLID FILMS, 2002, 407 (1-2) :26-31