Synthesis and crystal structure of Schiff bases based on AMTTO (AMTTO=4-amino-6-methyl-3-thio-3,4-dihydro-1,2,4-triazin-5(2H)-one)

被引：22

作者：

Tabatabaee, Maasoomeh ^{[1
]}

Ghassemzadeh, Mitra

Zarabi, Behnaz

Neumueller, Bernhard

机构：

[1] Islamic Azad Univ, Dept Chem, Yazd Branch, Tehran, Iran

[2] Chem & Chem Engn Res Ctr Iran, Tehran, Iran

[3] Univ Marburg, Fachbereich Chem, D-35032 Marburg, Germany

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 2006年 / 61卷 / 11期

关键词：

1,2,4-triazine; 1,2,4-triazole; Schiff base; microwave irradiation;

D O I：

10.1515/znb-2006-1116

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Reaction of 4-amino-6-methyl-3-thio-3,4-dihydro-1,2,4-triazin-5(2H)-one (1) with 2-methoxybenzaldehyde, 4-methoxybenzaldehyde, 2-pyridinecarbaldehyde, and 2,4-dichlorobenzaldehyde under classical heating and microwave irradiation in a solventfree system led to the corresponding imines (Schiff bases) 2-5. All synthesized compounds have been characterized by IR and NMR spectroscopy, mass spectrometry and by X-ray diffraction studies.

引用

页码：1421 / 1425

页数：5

共 24 条

[1] [Anonymous], 2015, Acta Crystallogr., V71, P3
[2] SYNTHESIS, CRYSTAL-STRUCTURE, AND SPECTROSCOPIC CHARACTERIZATION OF AF-DICHLORO-BD,EC-BIS(MU-[2-(1-METHYL-2-PIPERIDINYL)ETHANETHIOLATO]-S,N,MU-S) DIPALLADIUM(II)
BARRERA, H
VINAS, JM
FONTALTABA, M
SOLANS, X
[J]. POLYHEDRON, 1985, 4 (12) : 2027 - 2030
[3] Structural and spectral studies of thiosemicarbazones derived from 2-acetylthiophene
de Lima, GM
Neto, JL
Beraldo, H
Siebald, HGL
Duncalf, DJ
[J]. JOURNAL OF MOLECULAR STRUCTURE, 2002, 604 (2-3) : 287 - 291
[4] SYNTHESEN STICKSTOFFHALTIGER HETEROCYCLEN .27. UBER 1.2.4-TRIAZINE .1. DARSTELLUNG EINIGER NEUER S-TRIAZOLO(3.2-C)-AS-TRIAZINE
DORNOW, A
MENZEL, H
MARX, P
[J]. CHEMISCHE BERICHTE-RECUEIL, 1964, 97 (08): : 2173 - &
[5] SYNTHESIS AND CHARACTERIZATION OF SOME BIVALENT-METAL COMPLEXES OF ASYM-TRIAZINE AND ITS SCHIFF-BASES
DUBEY, SN
VAID, BK
[J]. SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY, 1991, 21 (09): : 1299 - 1311
[6] Structural and spectroscopic characteristics of aroylhydrazones derived from nicotinic acid hydrazide
Galic, N
Peric, B
Kojic-Prodic, B
Cimerman, Z
[J]. JOURNAL OF MOLECULAR STRUCTURE, 2001, 559 (1-3) : 187 - 194
[7] Synthesis, characterization of a novel 1,2,4-thiotriazine derivative (CAMTTO), and copper(I) and silver(I) complexes thereof (CAMTTO = {(4-[(4-chlorobenzylidene)-amino]-6-methyl-3-thioxo-[1,2,4]-triazin-3,4-dihydro(2H)-5-one)}
Ghassemzadeh, M
Tabatabaee, M
Pooramini, MM
Heravi, MM
Eslami, A
Neumüller, B
[J]. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2006, 632 (05): : 786 - 792
[8] Synthesis, characterization and crystal structures of new 1,2,4-triazole based Schiff-bases and their copper(I) complexes
Ghassemzadeh, M
Tabatabaee, M
Soleimani, S
Neumüller, B
[J]. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2005, 631 (10): : 1871 - 1876
[9] Synthesis and characterization of new AMTTO-imine-ligands and their silver(I) complexes:: crystal structures of TAMTTO, [Ag2(TAMMTO)4](NO3)2•4MeOH,[Ag(TAMTTO)(PPh3)2]NO3•1.5THF, [Ag(FAMTTO)(PPh3)2]NO3
Ghassemzadeh, M
Sharifi, A
Malakootikhah, J
Neumüller, B
Iravani, E
[J]. INORGANICA CHIMICA ACTA, 2004, 357 (08) : 2245 - 2252
[10] Ghassemzadeh M, 1998, Z ANORG ALLG CHEM, V624, P1969, DOI 10.1002/(SICI)1521-3749(1998120)624:12<1969::AID-ZAAC1969>3.0.CO

← 1 2 3 →