Effects of the fiber surface characteristics on the interfacial microstructure and mechanical properties of the KD SiC fiber reinforced SiC matrix composites

被引:73
作者
Liu, Haitao [1 ]
Cheng, Haifeng [1 ]
Wang, Jun [1 ]
Tang, Gengping [1 ]
Che, Renchao [1 ]
Ma, Qingsong [1 ]
机构
[1] Natl Univ Def Technol, Coll Aerosp & Mat Engn, Key Lab Adv Ceram Fiber & Composites, Changsha 410073, Peoples R China
来源
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 2009年 / 525卷 / 1-2期
关键词
SiCf/SiC composite; Precursor infiltration and pyrolysis (PIP); Surface characteristic; Interfacial microstructure; Mechanical property; SILICON-CARBIDE COMPOSITES; CERAMIC COMPOSITES; SIC/SIC COMPOSITES; RAMAN-SPECTROSCOPY; CRACKING; IMPROVEMENT; INTERPHASE; ROUGHNESS; BEHAVIOR;
D O I
10.1016/j.msea.2009.07.018
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
SiC fiber reinforced SiC matrix (SiCf/SiC) composites, employing two types of KD SiC fibers (from National University of Defense Technology, China) with different fiber surface characteristics as reinforcements, were fabricated by precursor infiltration and pyrolysis (PIP) process. The fiber surface characteristics were evaluated by SEM, XPS and Raman analysis. The effects of fiber surface characteristics on the interfacial microstructure and mechanical properties of the KD SiCf/SiC composites were investigated. The results show that the tensile strength of the KD-2 SiC fibers (with silicon-based oxide surface layers) is about 85% that of the KD-1 SiC fibers (with pyrocarbon (PyC) surface layers), but the flexural strength of the KD-2 SiCf/SiC composite is only around 15% that of the KD-1 SiCf/SiC composite. SEM, TEM and elemental mapping analysis show that the large strength difference between the two composites is ascribed to the interfacial microstructure and the degree of fiber damage, which are arising from the different fiber surface characteristics. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:121 / 127
页数:7
相关论文
共 24 条
[1]   Characterization of interfaces in C fiber-reinforced laminated C-SiC matrix composites [J].
Appiah, KA ;
Wang, ZL ;
Lackey, WJ .
CARBON, 2000, 38 (06) :831-838
[2]   FIBER-MATRIX DEBONDING EFFECTS ON CRACKING IN ALIGNED FIBER CERAMIC COMPOSITES [J].
BUDIANSKY, B ;
EVANS, AG ;
HUTCHINSON, JW .
INTERNATIONAL JOURNAL OF SOLIDS AND STRUCTURES, 1995, 32 (3-4) :315-328
[3]  
Chu ZY, 2004, J WUHAN UNIV TECHNOL, V19, P36
[4]   Study of the pyrolysis process of an hybrid CH3SiO1.5 gel into a SiCO glass [J].
Das, Gobind ;
Bettotti, Paolo ;
Ferraioli, Luigi ;
Raj, Rishi ;
Mariotto, Gino ;
PaveSib, Lorenzo ;
Soraru, Gian Domenico .
VIBRATIONAL SPECTROSCOPY, 2007, 45 (01) :61-68
[5]   INTERFACE DEBONDING AND FIBER CRACKING IN BRITTLE MATRIX COMPOSITES [J].
EVANS, AG ;
HE, MY ;
HUTCHINSON, JW .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1989, 72 (12) :2300-2303
[6]   THE PHYSICS AND MECHANICS OF FIBER-REINFORCED BRITTLE-MATRIX COMPOSITES [J].
EVANS, AG ;
ZOK, FW .
JOURNAL OF MATERIALS SCIENCE, 1994, 29 (15) :3857-3896
[7]   Non-destructive mechanical characterization of SiC fibers by Raman spectroscopy [J].
Gouadec, G ;
Colomban, P .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2001, 21 (09) :1249-1259
[8]   Improvement of mechanical properties of SiC/SiC composites by various surface treatments of fibers [J].
Hinoki, T ;
Yang, W ;
Nozawa, T ;
Shibayama, T ;
Katoh, Y ;
Kohyama, A .
JOURNAL OF NUCLEAR MATERIALS, 2001, 289 (1-2) :23-29
[9]   Interfacial smear debonding problems in fiber-reinforced ceramic composites [J].
Hsueh, CH ;
Becher, PF .
ACTA MATERIALIA, 1998, 46 (09) :3237-3245
[10]   Mechanical properties of SiC/SiC composite with magnesium-silicon oxide interphase [J].
Igawa, N. ;
Taguchi, T. ;
Yamada, R. ;
Ishii, Y. ;
Jitsukawa, S. .
JOURNAL OF NUCLEAR MATERIALS, 2007, 367 :725-729