Preparation of ZrO2:Tb via microwave hydrothermal method

被引:0
|
作者
Kaszewski, Jaroslaw [1 ]
Lojkowski, Witold [2 ]
Narkiewicz, Urszula [1 ]
机构
[1] W Pomeranian Univ Technol, Inst Chem & Environm Engn, PL-70322 Szczecin, Poland
[2] Polish Acad Sci, Inst High Pressure Phys, PL-01142 Warsaw, Poland
关键词
zirconia; terbium; microwave; hydrothermal; NANOCRYSTALLINE ZIRCONIA; SUPERCRITICAL WATER; CRYSTALLITE SIZE; NANOPARTICLES; STABILIZATION;
D O I
暂无
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
Terbium doped zirconium dioxide was successfully synthesized using microwave hydrothermal method. The powder is strongly agglomerated and has mean crystallite size around 6 nm. The density of obtained powders is significantly lower than density of bulk zirconium dioxide indicating the existence of zirconium and dopant hydroxides remaining after the hydrothermal process. The effect of terbium on morphology, phase composition, specific surface area and density of the samples was determined.
引用
收藏
页码:773 / 779
页数:7
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