Preparation of ZrO2:Tb via microwave hydrothermal method

被引:0
|
作者
Kaszewski, Jaroslaw [1 ]
Lojkowski, Witold [2 ]
Narkiewicz, Urszula [1 ]
机构
[1] W Pomeranian Univ Technol, Inst Chem & Environm Engn, PL-70322 Szczecin, Poland
[2] Polish Acad Sci, Inst High Pressure Phys, PL-01142 Warsaw, Poland
关键词
zirconia; terbium; microwave; hydrothermal; NANOCRYSTALLINE ZIRCONIA; SUPERCRITICAL WATER; CRYSTALLITE SIZE; NANOPARTICLES; STABILIZATION;
D O I
暂无
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
Terbium doped zirconium dioxide was successfully synthesized using microwave hydrothermal method. The powder is strongly agglomerated and has mean crystallite size around 6 nm. The density of obtained powders is significantly lower than density of bulk zirconium dioxide indicating the existence of zirconium and dopant hydroxides remaining after the hydrothermal process. The effect of terbium on morphology, phase composition, specific surface area and density of the samples was determined.
引用
收藏
页码:773 / 779
页数:7
相关论文
共 50 条
  • [1] Preparation of Nano-ZrO2 powder via a microwave-assisted hydrothermal method
    Guo, Mingyi
    Wang, Guangxin
    Zhao, Yunchao
    Li, Haitao
    Tang, Kun
    Zhao, Yibo
    Burgess, Kevin
    CERAMICS INTERNATIONAL, 2021, 47 (09) : 12425 - 12432
  • [2] Synthesis of ZrO2 Nanoparticles by Hydrothermal Treatment
    Machmudah, Siti
    Widiyastuti, W.
    Prastuti, Okky Putri
    Nurtono, Tantular
    Winardi, Sugeng
    Wahyudiono
    Kanda, Hideki
    Goto, Motonobu
    5TH NANOSCIENCE AND NANOTECHNOLOGY SYMPOSIUM (NNS2013), 2014, 1586 : 166 - 172
  • [3] Preparation of amorphous ZrO2 powders by hydrothermal-assisted sol-gel method
    Dan, Hui
    Chen, Li
    Li, Zhen
    He, Xinmiao
    Ding, Yi
    INORGANIC CHEMISTRY COMMUNICATIONS, 2022, 138
  • [4] Preparation of a CeO2-nanoparticle thermal radiation shield coating on ZrO2 fibers via a hydrothermal method
    Gan, Xinzhu
    Yu, Zhichao
    Yuan, Kangkang
    Xu, Chonghe
    Wang, Xinqiang
    Zhu, Luyi
    Zhang, Guanghui
    Xu, Dong
    CERAMICS INTERNATIONAL, 2017, 43 (16) : 14183 - 14191
  • [5] Optimization of experimental parameters to the formation of ZrO2 phase via hydrothermal method
    Yang, H. Z.
    Han, L. Z.
    Zhao, L. A.
    Zhi, Z. Z.
    Ji, Y.
    ADVANCES IN ENGINEERING MATERIALS AND APPLIED MECHANICS, 2016, : 11 - 15
  • [6] Preparation of ZrO2 in SiC coating via hydrothermal method and sintering process onto carbon/carbon composite
    Mao, Zu-Li
    Yang, Li
    Wu, Jie
    MATERIALS EXPRESS, 2021, 11 (12) : 1997 - 2003
  • [7] Synthesis of Elusive Monoclinic ZrO2 Nanostructures via Hydrothermal Treatment
    Thakur, Sakshi
    Sareen, Shweta
    Verma, Meenakshi
    Kaur, Kirtanjot
    Mutreja, Vishal
    JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS, 2024, 34 (01) : 61 - 78
  • [8] Preparation of Nanocrystalline ZrO2 Powder via A Chemical Route
    Septawendar, Rifki
    Sutardi, Suhanda
    Purwasasmita, Bambang Sunendar
    Edwin, Frank
    JOURNAL OF THE AUSTRALIAN CERAMIC SOCIETY, 2012, 48 (01) : 12 - 20
  • [9] Luminescent properties of ZrO2:Tb nanoparticles for applications in neuroscience
    Slonska, A.
    Kaszewski, J.
    Wolska-Kornio, E.
    Witkowski, B.
    Wachnicki, L.
    Mijowska, E.
    Karakitsou, V.
    Gajewski, Z.
    Godlewski, M.
    Godlewski, M. M.
    OPTICAL MATERIALS, 2016, 59 : 96 - 102
  • [10] Aqueous ZrO2 and YSZ Colloidal Systems through Microwave Assisted Hydrothermal Synthesis
    Vernieuwe, Kenny
    Lommens, Petra
    Martins, Jose C.
    Van den Broeck, Freya
    Van Driessche, Isabel
    De Buysser, Klaartje
    MATERIALS, 2013, 6 (09) : 4082 - 4095