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1H, 13C and 15N NMR and GIAO CPHF calculations on two quinoacridinium salts
被引：0
|作者：
Jaroszewska-Manaj, J
Maciejewska, D
Wawer, I
机构：
[1] Med Univ Warsaw, Fac Pharm, Dept Phys Chem, PL-02097 Warsaw, Poland
[2] Univ Warsaw, Dept Chem, PL-02093 Warsaw, Poland
关键词：
NMR;
H-1;
C-13;
N-15;
2D NMR (HMBC;
HSQC;
HMQC);
GIAO CPHF calculations;
quinoacridine salts;
synthesis;
D O I：
10.1002/1097-458X(200006)38:6<482::AID-MRC677>3.0.CO;2-P
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The complete H-1,C-13 and N-15 NMR assignments of two closely related quinoacridinium salts, 8,13-diethyl-6-methy1-8H-quino[4,3,2-kl]acridinium iodide and, 8,13-diethyl-3,6,11-trimethyl-8H-quino[4,3,2-kl]acridinium iodide, are described. The multinuclear 1D NMR and 2D shift-correlated NMR techniques HMQC, HSQC and HMBC were applied, accompanied by ab initio GIAO CPHF calculations of shielding constants. Copyright (C) 2000 John Wiley & Sons, Ltd.
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页码：482 / 485
页数：4
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