Magnetic Properties of Poly(trimethylene terephthalate-block-Poly(tetramethylene oxide) Copolymer Nanocomposites Reinforced by Graphene Oxide-Fe3O4 Hybrid Nanoparticles

被引:4
作者
Szymczyk, Anna [1 ]
Paszkiewicz, Sandra [2 ]
Typek, Janusz [1 ]
Spitalsky, Zdenko [3 ]
Janowska, Izabela [4 ,5 ]
Zolnierkiewicz, Grzegorz [1 ]
Guskos, Nikos [1 ]
机构
[1] West Pomeranian Univ Technol, Inst Phys, Piastow Ave 48, PL-70310 Szczecin, Poland
[2] West Pomeranian Univ Technol, Inst Mat Sci & Engn, Piastow Ave 19, PL-70310 Szczecin, Poland
[3] Slovak Acad Sci, Inst Polymer, Dubravska Cesta 9, Bratislava 84541, Slovakia
[4] CNRS, Inst Chem & Proc Energy Environm & Hlth ICPEES, 25 Rue Becquerel, F-67087 Strasbourg 2, France
[5] Univ Strasbourg, 25 Rue Becquerel, F-67087 Strasbourg 2, France
来源
PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE | 2019年 / 216卷 / 23期
关键词
graphene oxide-Fe3O4 nanoparticles hybrid; magnetic properties; phase structures; polyester thermoplastic elastomers; polymer nanocomposites; FERROMAGNETIC-RESONANCE; REUSABLE CATALYST; ANISOTROPY CONSTANTS; VERWEY TRANSITION; GREEN SYNTHESIS; LEAF EXTRACT; FMR SPECTRA; SURFACE; FE3O4; REDUCTION;
D O I
10.1002/pssa.201900402
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Thermoplastic elastomeric nanocomposites based on poly(trimethylene terephthalate-block-poly(tetramethylene oxide) copolymer (PTT-PTMO) and graphene oxide (GO)-Fe3O4 nanoparticles hybrid are prepared by in situ polymerization. Superparamagnetic GO-Fe3O4 hybrid nanoparticles before introducing to elastomeric matrix are characterized by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM). The effect of loading (0.3 and 0.5 wt%) of GO-Fe3O4 nanoparticle hybrid on the phase structure, tensile, and magnetic properties of synthesized nanocomposites is investigated. The phase structure of nanocomposites is evaluated by differential scanning calorimetry (DSC) and dynamic mechanical thermal analysis (DMTA). Dispersion of GO-Fe3O4 nanoparticles in elastomeric matrix is evaluated by transmission electron microscopy (TEM). Magnetic properties of GO-Fe3O4 nanoparticle hybrid and nanocomposites with their content are characterized using two different techniques: direct current superconducting quantum interference device (dc SQUID) magnetization measurements as a function of temperature (from 2 to 300 K) and external magnetic field and ferromagnetic resonance (FMR) at microwave frequency.
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页数:16
相关论文
共 83 条
[1]   Characterization of single-core magnetite nanoparticles for magnetic imaging by SQUID relaxometry [J].
Adolphi, Natalie L. ;
Huber, Dale L. ;
Bryant, Howard C. ;
Monson, Todd C. ;
Fegan, Danielle L. ;
Lim, JitKang ;
Trujillo, Jason E. ;
Tessier, Trace E. ;
Lovato, Debbie M. ;
Butler, Kimberly S. ;
Provencio, Paula P. ;
Hathaway, Helen J. ;
Majetich, Sara A. ;
Larson, Richard S. ;
Flynn, Edward R. .
PHYSICS IN MEDICINE AND BIOLOGY, 2010, 55 (19) :5985-6003
[2]   Magnetization enhancement in magnetite nanoparticles capped with alginic acid [J].
Andrzejewski, Bartlomiej ;
Bednarski, Waldemar ;
Kazmierczak, Malgorzata ;
Lapinski, Andrzej ;
Pogorzelec-Glaser, Katarzyna ;
Hilczer, Bozena ;
Jurga, Stefan ;
Nowaczyk, Grzegorz ;
Zaleski, Karol ;
Matczak, Michal ;
Leska, Boguslawa ;
Pankiewicz, Radoslaw ;
Kepinski, Leszek .
COMPOSITES PART B-ENGINEERING, 2014, 64 :147-154
[3]   Green synthesis of Pd/RGO/Fe3O4 nanocomposite using Withania coagulans leaf extract and its application as magnetically separable and reusable catalyst for the reduction of 4-nitrophenol [J].
Atarod, Monireh ;
Nasrollahzadeh, Mahmoud ;
Sajadi, S. Mohammad .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2016, 465 :249-258
[4]   Green synthesis of a Cu/reduced graphene oxide/Fe3O4 nanocomposite using Euphorbia wallichii leaf extract and its application as a recyclable and heterogeneous catalyst for the reduction of 4-nitrophenol and rhodamine B [J].
Atarod, Monireh ;
Nasrollahzadeh, Mahmoud ;
Sajadi, S. Mohammad .
RSC ADVANCES, 2015, 5 (111) :91532-91543
[5]   EPR evidence of antiferromagnetic ordering in single-layer graphene [J].
Augustyniak-Jablokow, Maria A. ;
Tadyszak, Krzysztof ;
Mackowiak, Mariusz ;
Yablokov, Yurii V. .
PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS, 2011, 5 (08) :271-273
[6]   Surface and exchange anisotropy fields in MnFe2O4 nanoparticles:: Size and temperature effects [J].
Bakuzis, AF ;
Morais, PC ;
Pelegrini, F .
JOURNAL OF APPLIED PHYSICS, 1999, 85 (10) :7480-7482
[7]   Enhanced Magnetism in Highly Ordered Magnetite Nanoparticle-Filled Nanohole Arrays [J].
Binh Duong ;
Khurshid, Hafsa ;
Gangopadhyay, Palash ;
Devkota, Jagannath ;
Stojak, Kristen ;
Srikanth, Hariharan ;
Tetard, Laurene ;
Norwood, Robert A. ;
Peyghambarian, N. ;
Manh-Huong Phan ;
Thomas, Jayan .
SMALL, 2014, 10 (14) :2840-2848
[8]  
Bodziony T, 2005, MATER SCI-POLAND, V23, P1055
[9]  
Bodziony T, 2004, REV ADV MATER SCI, V8, P86
[10]   Nanocrystalline iron oxide based electroactive materials in lithium ion batteries: the critical role of crystallite size, morphology, and electrode heterostructure on battery relevant electrochemistry [J].
Bruck, Andrea M. ;
Cama, Christina A. ;
Gannett, Cara N. ;
Marschilok, Amy C. ;
Takeuchi, Esther S. ;
Takeuchi, Kenneth J. .
INORGANIC CHEMISTRY FRONTIERS, 2016, 3 (01) :26-40