Magnetic Properties of Poly(trimethylene terephthalate-block-Poly(tetramethylene oxide) Copolymer Nanocomposites Reinforced by Graphene Oxide-Fe3O4 Hybrid Nanoparticles

被引：4
作者：
Szymczyk, Anna [1 ]
Paszkiewicz, Sandra [2 ]
Typek, Janusz [1 ]
Spitalsky, Zdenko [3 ]
Janowska, Izabela [4 ,5 ]
Zolnierkiewicz, Grzegorz [1 ]
Guskos, Nikos [1 ]
机构：
[1] West Pomeranian Univ Technol, Inst Phys, Piastow Ave 48, PL-70310 Szczecin, Poland
[2] West Pomeranian Univ Technol, Inst Mat Sci & Engn, Piastow Ave 19, PL-70310 Szczecin, Poland
[3] Slovak Acad Sci, Inst Polymer, Dubravska Cesta 9, Bratislava 84541, Slovakia
[4] CNRS, Inst Chem & Proc Energy Environm & Hlth ICPEES, 25 Rue Becquerel, F-67087 Strasbourg 2, France
[5] Univ Strasbourg, 25 Rue Becquerel, F-67087 Strasbourg 2, France
来源：
PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE | 2019年 / 216卷 / 23期
关键词：
graphene oxide-Fe3O4 nanoparticles hybrid; magnetic properties; phase structures; polyester thermoplastic elastomers; polymer nanocomposites; FERROMAGNETIC-RESONANCE; REUSABLE CATALYST; ANISOTROPY CONSTANTS; VERWEY TRANSITION; GREEN SYNTHESIS; LEAF EXTRACT; FMR SPECTRA; SURFACE; FE3O4; REDUCTION;
D O I：
10.1002/pssa.201900402
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Thermoplastic elastomeric nanocomposites based on poly(trimethylene terephthalate-block-poly(tetramethylene oxide) copolymer (PTT-PTMO) and graphene oxide (GO)-Fe3O4 nanoparticles hybrid are prepared by in situ polymerization. Superparamagnetic GO-Fe3O4 hybrid nanoparticles before introducing to elastomeric matrix are characterized by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM). The effect of loading (0.3 and 0.5 wt%) of GO-Fe3O4 nanoparticle hybrid on the phase structure, tensile, and magnetic properties of synthesized nanocomposites is investigated. The phase structure of nanocomposites is evaluated by differential scanning calorimetry (DSC) and dynamic mechanical thermal analysis (DMTA). Dispersion of GO-Fe3O4 nanoparticles in elastomeric matrix is evaluated by transmission electron microscopy (TEM). Magnetic properties of GO-Fe3O4 nanoparticle hybrid and nanocomposites with their content are characterized using two different techniques: direct current superconducting quantum interference device (dc SQUID) magnetization measurements as a function of temperature (from 2 to 300 K) and external magnetic field and ferromagnetic resonance (FMR) at microwave frequency.
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页数：16
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