Preparation of Ni-W-Si3N4 composite coatings and evaluation of their scratch resistance properties

被引:53
作者
Gyawali, Gobinda [1 ]
Joshi, Bhupendra [1 ]
Tripathi, Khagendra [1 ]
Lee, Soo Wohn [1 ]
机构
[1] Sun Moon Univ, Res Ctr Eco Multifunct Nano Mat, Asan, South Korea
基金
新加坡国家研究基金会;
关键词
Ni-W-Si3N4; Alloy; Microhardness; Scratch; NI-W COATINGS; ELECTRODEPOSITION; NANOCRYSTALLINE; MICROSTRUCTURE; DEPOSITION; BEHAVIOR; ALLOYS;
D O I
10.1016/j.ceramint.2015.10.153
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this study, Ni-W-Si3N4 nanocomposite coatings have been prepared by codeposition of Si3N4 nanoparticles into Ni-W alloy coatings having different W contents. The surface morphology and elemental contents in the alloy composite coatings have been analyzed by scanning electron microscopy coupled with EDS. Structure and phase composition were evaluated by using X-ray diffraction (XRD). Progressive type of scratch test was carried out by the scratch tester using a diamond indenter. Results indicated that Vickers microhardness of the Ni-W-Si3N4 composite coatings is found to be higher in comparison to the corresponding Ni-W coatings. In addition, a small increase in Vickers microhardness was observed in Ni-W coatings with higher content of tungsten. Apart from that, a significant influence had been found on scratch resistance properties with the codeposition of Si3N4 and variation of W contents in Ni-W-Si3N4 nanocomposite coatings. Ni-W-Si3N4 nanocomposite with 12.7 at% W and 2.1 wt% Si3N4 has shown improved scratch resistance among others. (C) 2015 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:3497 / 3503
页数:7
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