Preparation of dense BaTiO3 ceramic fiber by a sol-gel and solvothermal route

被引:0
作者
Liu Yong [1 ]
Lu Qi-Fang
Chen Chang-Long
Chen Dai-Rong
Jiao Xiu-Ling
机构
[1] Shandong Univ, Dept Chem, Jinan 250100, Peoples R China
[2] Shandong Inst Light Ind, Dept Mat, Jinan 250100, Peoples R China
[3] Jinan Univ, Dept Chem, Jinan 250022, Peoples R China
关键词
BaTiO3; ceramic fiber; sol-gel; solvothermal;
D O I
暂无
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Dense BaTiO3 ceramic fibers were obtained by solvothermal treatment of the green gel fibers, which were drawn from a sol using barium acetate hydrate and catechol-complexed titanium isoproposide as starting materials, at 180 degrees C for 12h in n-hexane following a heat process to 1100 degrees C with a heating rate of 1 degrees C/min for crystallization. The as-synthesized BaTiO3 ceramic fibers were characterized by X-ray diffraction (XRD), Infrared (IR) spectra and scanning electron microscope (SEM) techinques.
引用
收藏
页码:1487 / 1490
页数:4
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