(2E)-2-(1-Methylpiperidin-2-ylidene)-1-phenyl-ethanone

被引：3

作者：

Lemmerer, Andreas ^{[1
]}

Michael, Joseph P. ^{[1
]}

Pienaar, Daniel P. ^{[1
]}

Sannasy, Desigan ^{[1
]}

机构：

[1] Univ Witwatersrand, Sch Chem, Inst Mol Sci, ZA-2050 Johannesburg, South Africa

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷

关键词：

D O I：

10.1107/S160053680605152X

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C14H17NO, the piperidine ring is in a half-chair conformation. The molecules are linked into C( 7) chains by an intermolecular C - H center dot center dot center dot O hydrogen bond.

引用

页码：O98 / O99

页数：2

共 14 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2]

[Anonymous], 1999, J. Appl. Crystallogr, DOI [DOI 10.1107/S0021889899006020, 10.1107/S0021889899006020]

[3] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[4]

BRANDENBURG K, 1999, DIAMOND VERSION 2 1E

[5]

*BRUK AXS INC, 1998, SMART NT VERS 5 050

[6]

*BRUK AXS INC, 1999, SAINT PLUS VERS 6 02

[7] GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].

CREMER, D ;

POPLE, JA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358

[8] GRAPH-SET ANALYSIS OF HYDROGEN-BOND PATTERNS IN ORGANIC-CRYSTALS [J].

ETTER, MC ;

MACDONALD, JC ;

BERNSTEIN, J .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1990, 46 :256-262

[9]

Farrugia L.J., 1997, J APPL CRYSTALLOGR, V30, P565

[10] (+/-)-Sedamine and (+/-)-allosedamine by reduction of N-methyl-2-phenacylidenepiperidine [J].

Ghiaci, M ;

Adibi, M .

ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1996, 28 (04) :474-477

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