Identification of aroma active compounds in cardboard using Solid Phase Microextraction (SPME) coupled with GC-MS and GC-Olfactometry

被引:0
作者
Leitner, E [1 ]
Pfannhauser, W [1 ]
机构
[1] Graz Univ Technol, Dept Food Chem, Inst Bio & Food Chem, A-8010 Graz, Austria
来源
FRONTIERS OF FLAVOUR SCIENCE | 2000年
关键词
D O I
暂无
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
A rapid method using Solid Phase Microextraction (SPME) was developed for the identification and determination of odour active compounds in cardboard samples. Several fibers were tested under different conditions (time, temperature) in order to optimize the sensitivity of the method. Finally, a 75 mum Carboxen fiber was selected for the enrichment of the volatile fraction. The fiber was exposed to the headspace of the cardboard sample for 50 minutes at 50degreesC. The compounds were identified using GC-MS and a retention index database. The odour active compounds were additionally identified by gas chromatography coupled to a sniffing port (GC-Olfactometry). Several aroma active compounds, mainly saturated and unsaturated aldehydes could be identified using this method.
引用
收藏
页码:74 / 78
页数:5
相关论文
共 50 条
[21]   GC-MS and GC-olfactometry analysis of aroma compounds in a representative organic aroma extract from cured vanilla (Vanilla planifolia G. Jackson) beans [J].
Perez-Silva, A. ;
Odoux, E. ;
Brat, P. ;
Ribeyre, F. ;
Rodriguez-Jimenes, G. ;
Robles-Olvera, V. ;
Garcia-Alvarado, M. A. ;
Gunata, Z. .
FOOD CHEMISTRY, 2006, 99 (04) :728-735
[22]   Analysis of the headspace aroma compounds of the seeds of the Cameroonian "garlic plant" Hua gabonii using SPME/GC/FID, SPME/GC/MS and olfactometry [J].
Leopold Jirovetz ;
Gerhard Buchbauer ;
Martin Ngassoum ;
Margit Geissler .
European Food Research and Technology, 2002, 214 :212-215
[23]   Analysis of the headspace aroma compounds of the seeds of the Cameroonian "garlic plant" Hua gabonii using SPME/GC/FID, SPME/GC/MS and olfactometry [J].
Jirovetz, L ;
Buchbauer, G ;
Ngassoum, MB ;
Geissler, M .
EUROPEAN FOOD RESEARCH AND TECHNOLOGY, 2002, 214 (03) :212-215
[24]   Determination of vanillin in orange, grapefruit, tangerine, lemon, and lime juices using GC-olfactometry and GC-MS/MS [J].
Goodner, KL ;
Jella, P ;
Rouseff, RL .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2000, 48 (07) :2882-2886
[25]   Comparative study on volatile compounds and taste components of various citrus cultivars using electronic sensors, GC-MS, and GC-olfactometry [J].
Jo, Seong Min ;
Hong, Seong Jun ;
Yoon, Sojeong ;
Jeong, Hyangyeon ;
Youn, Moon Yeon ;
Shin, Eui-Cheol .
FOOD SCIENCE AND BIOTECHNOLOGY, 2024, 33 (08) :1825-1837
[26]   Determination of triazines and amides in water using solid phase microextraction coupled with GC-MS [J].
R. Hu ;
D. Elia ;
J. -M. Berthion ;
S. Poliak .
Chromatographia, 2001, 53 :306-310
[27]   Determination of triazines and amides in water using solid phase microextraction coupled with GC-MS [J].
Hu, R ;
Elia, D ;
Berthion, JM ;
Poliak, S .
CHROMATOGRAPHIA, 2001, 53 (5-6) :306-310
[28]   Characterisation of aroma volatiles in carrots using GC-Olfactometry and aroma extract dilution [J].
Edelenbos, M ;
Christensen, LP ;
Kjeldsen, F .
Flavour Research at the Dawn of the Twenty-First Century, 2003, :588-591
[29]   Optimization of Headspace Solid-Phase Micro-extraction (HS-SPME) for Analyzing Soy Sauce Aroma Compounds via Coupling with Direct GC-Olfactometry (D-GC-O) and Gas Chromatography-Mass Spectrometry (GC-MS) [J].
Yunzi Feng ;
Guowan Su ;
Dongxiao Sun-Waterhouse ;
Yu Cai ;
Haifeng Zhao ;
Chun Cui ;
Mouming Zhao .
Food Analytical Methods, 2017, 10 :713-726
[30]   Optimization of Headspace Solid-Phase Micro-extraction (HS-SPME) for Analyzing Soy Sauce Aroma Compounds via Coupling with Direct GC-Olfactometry (D-GC-O) and Gas Chromatography-Mass Spectrometry (GC-MS) [J].
Feng, Yunzi ;
Su, Guowan ;
Sun-Waterhouse, Dongxiao ;
Cai, Yu ;
Zhao, Haifeng ;
Cui, Chun ;
Zhao, Mouming .
FOOD ANALYTICAL METHODS, 2017, 10 (03) :713-726