2,2-dichloro-1-(4-ethoxyphenyl)cyclopropanyl piperidin-1-yl ketone

被引:2
作者
Sun, Na-Bo
Shen, De-Long [1 ]
Zheng, Ren-Hua
Tan, Cheng-Xia
Weng, Jian-Quan
机构
[1] Zhejiang Univ Technol, Coll Chem Engn & Mat Sci, Hangzhou 310014, Peoples R China
[2] Taizhou Univ, Sch Pharmaceut & Chem Engn, Linhai 317000, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2006年 / 62卷
关键词
D O I
10.1107/S160053680604743X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C17H21Cl2NO2, a cyclopropane derivative related to the insecticide cycloprothrin, was prepared from piperidine and 2,2-dichloro-1-(4-ethoxyphenyl) cyclopropanecarbonyl chloride. The six-membered piperidine ring has a chair conformation. The orientation of the carbonyl group relative to the cyclopropane ring may be described by the torsion angle X-C-C=O of -98.3 degrees, where X is the centroid of the cyclopropane ring.
引用
收藏
页码:O5679 / O5680
页数:2
相关论文
共 9 条
[1]   COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92 [J].
ALTOMARE, A ;
CASCARANO, G ;
GIACOVAZZO, C ;
GUAGLIARDI, A .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) :343-350
[2]   CRYSTALS version 12: software for guided crystal structure analysis [J].
Betteridge, PW ;
Carruthers, JR ;
Cooper, RI ;
Prout, K ;
Watkin, DJ .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :1487-1487
[3]   GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].
CREMER, D ;
POPLE, JA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358
[5]  
Higashi T., 1995, ABSCOR
[6]   SYNTHESIS AND BIOLOGICAL-ACTIVITY OF DDT-PYRETHROID INSECTICIDES [J].
HOLAN, G ;
JOHNSON, WM ;
VIRGONA, CT ;
WALSER, RA .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1986, 34 (03) :520-524
[7]  
Larson A.C., 1970, CRYSTALLOGRAPHIC COM, P291
[8]  
*MSC RIG, 2004, CRYST STRUCT VERS 3
[9]  
Rigaku, 1998, PROCESS AUTO