Triplet NOAH supersequences optimised for small molecule structure characterisation

被引：20
|
作者：
Claridge, Tim D. W. [1 ]
Mayzel, Maksim [2 ]
Kupce, Eriks [3 ]
机构：
[1] Univ Oxford, Dept Chem, Chem Res Lab, Mansfield Rd, Oxford OX1 3TA, England
[2] Bruker BioSpin AG, MRS Div, Applicat Sci CH, Fallanden, Switzerland
[3] Bruker UK Ltd, Adv Applicat Dev, Coventry, W Midlands, England
来源：
MAGNETIC RESONANCE IN CHEMISTRY | 2019年 / 57卷 / 11期
关键词：
COSY; HMBC; HSQC; MFA; NMR; NOAH; NOESY; NUS; ROESY; TOCSY; NMR-SPECTROSCOPY; MULTIDIMENSIONAL NMR; ACQUISITION;
D O I：
10.1002/mrc.4887
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A series of NMR supersequences are presented for the time-efficient structure characterisation of small molecules in the solution state. These triplet sequences provide HMBC, HSQC, and one homonuclear correlation experiment of choice according to the NMR by Ordered Acquisition using H-1 detection principle. The experiments are demonstrated to be compatible with non-uniform sampling schemes and may be acquired and processed under full automation.
引用
收藏
页码：946 / 952
页数：7
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