Thermal Investigation of Al2O3 Thin Films for Application in Cutting Operations

被引:10
作者
Bobzin, Kirsten [1 ]
Bagcivan, Nazlim [1 ]
Immich, Philipp [1 ]
Ewering, Mara [1 ]
机构
[1] Rhein Westfal TH Aachen, Surface Engn Inst, D-52056 Aachen, Germany
关键词
Bipolar pulse - Bond coats - Cutting operations - Domain size - Energy dispersive X ray spectroscopy - Oxidation stability - Rectangular pulse;
D O I
10.1002/adem.200800421
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A study was conducted for thermal investigation of Al2O 3 thin films for application in cutting operations. Coated alumina samples were annealed from 600-1200 °C under vacuum for 4 hours and for another 600-1200 ° C in air for 4 hours. The samples were annealed under these conditions to prove the oxidation stability of the coatings under cutting operation conditions. The samples were also analyzed using X-ray diffractometry (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), nanoindentation, and domain size evolution. The investigated coatings were deposited using four cathodes in two-by-two cathode arrangement, which were pulsed in a bipolar pulse mode using a rectangular pulse having a frequency of 18.51 kHz. A TiAlN bond coat was also applied to assure significant adhesion of the coating.
引用
收藏
页码:590 / 594
页数:5
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