Synthesis and Crystal Structure of a Depside Derivative 2-(2-Methoxy-2-oxoethyl)phenyl 2-(3,4-Dimethoxyphenyl)acetate

被引：2

作者：

Lv, Peng-Cheng ^{[1
,2
]}

Wang, Kai-Rui ^{[1
]}

Mao, Wen-Jun ^{[1
]}

Fang, Rui-Qin ^{[1
]}

Chen, Jin ^{[1
]}

Xiong, Jing ^{[1
]}

Zhu, Hai-Liang ^{[1
,2
]}

机构：

[1] Nanjing Univ, State Key Lab Pharmaceut Biotechnol, Nanjing 210093, Peoples R China

[2] Anhui Univ Technol, Key Lab, Anhui Educ Dept, Maanshan 243002, Peoples R China

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2009年 / 39卷 / 12期

基金：

中国国家自然科学基金; 安徽省自然科学基金;

关键词：

Synthesis; Crystal structure; Depside; METABOLITES; INHIBITION;

D O I：

10.1007/s10870-009-9622-0

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

A depside derivative, 2-(2-methoxy-2-oxoethyl) phenyl 2-(3,4-dimethoxyphenyl) acetate (3), was synthesized through a facile approach in high yields. Its structure was confirmed by H-1 NMR, C-13 NMR, ESI mass spectra, elemental analyses and X-ray single crystal diffraction study. Crystal structure analysis revealed that compound 3 crystallized in the monoclinic, space group P2(1)/c with the following unit cell parameters: a = 10.173(2) angstrom, b = 10.459(2) angstrom, c = 16.516(3) angstrom, alpha = 90 degrees, beta = 102.30(3)degrees, gamma = 90 degrees, V = 1717.0(6) angstrom(3), Z = 4.

引用

页码：927 / 930

页数：4

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