Oxidation of 3,4-dihydropyrimidin-2(1H)-ones with nitrosonium (NO+)

被引：10
|
作者：
Liang, Rui Rui [1 ]
Wu, Guai Li [1 ]
Wu, Wen Tao [1 ]
Wu, Long Min [1 ]
机构：
[1] Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2009年 / 20卷 / 10期
基金：
中国国家自然科学基金;
关键词：
Dihydropyrimidinone; Nitrosonium; Oxidation; PHENYL 2,4,6-TRINITROPHENYL ETHER; AROMATIC-SUBSTITUTION REACTIONS; NONPOLAR APROTIC-SOLVENT; SOLID-PHASE SYNTHESIS; NITRIC-OXIDE; HANTZSCH 1,4-DIHYDROPYRIDINES; ELECTROCHEMICAL OXIDATION; PYRIMIDINE; BIGINELLI; DIHYDROPYRIMIDINONES;
D O I：
10.1016/j.cclet.2009.04.039
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
3, 4-Dihydropyrimidin-2(1H)-ones (DHPMs) were oxidized with 1.2 equiv. of nitrosonium tetrafluoroborate (NO+BF4-) to pyrimidin-2(1H)-ones in acetonitrile at room temperature in high yields. (C) 2009 Long Min Wu. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
引用
收藏
页码：1183 / 1186
页数：4
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