(2-Aminoethoxy)bis(2-thienyl)boron

被引:4
作者
Low, JN [1 ]
Musgrave, O
Wardell, J
机构
[1] Univ Dundee, Dept Appl Phys & Elect & Mech Engn, Dundee DD1 4HN, Scotland
[2] Univ Aberdeen, Dept Chem, Old Aberdeen AB24 3UE, Scotland
来源
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2000年 / 56卷
关键词
D O I
10.1107/S0108270100000482
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In the five-membered ring in the title compound, (2-aminoethoxy)bis(2-thienyl)boron, C10H12BNOS2, the B atom is four-coordinate with dimensions N-B 1.654 (3), O-B 1.479 (3), and C-B 1.606 (3) and 1.609 (3) Angstrom. An intermolecular hydrogen bond between an amino H atom and the ethoxy O atom links the molecules into infinite chains along the a axis. Only one of the two amino H atoms is involved in hydrogen bonding because there is only the one acceptor atom, the ethoxy O atom, and the molecular geometry precludes formation of a second hydrogen bond by the second amino H atom.
引用
收藏
页码:E63 / E63
页数:1
相关论文
共 8 条
[1]   Outlier treatment in data merging [J].
Blessing, RH .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1997, 30 :421-426
[2]   AN EMPIRICAL CORRECTION FOR ABSORPTION ANISOTROPY [J].
BLESSING, RH .
ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :33-38
[3]  
COUTTS IG, 1970, J CHEM SOC C, P225
[4]  
FERGUSON G, 1999, PRPKAPPA
[5]  
*NON BV, 1997, KAPP SERV SOFTW
[6]   Processing of X-ray diffraction data collected in oscillation mode [J].
Otwinowski, Z ;
Minor, W .
MACROMOLECULAR CRYSTALLOGRAPHY, PT A, 1997, 276 :307-326
[7]  
Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR
[8]  
Spek A. L., 1999, PLATON