Water-compatible molecularly imprinted polymers for selective solid phase extraction of dencichine from the aqueous extract of Panax notoginseng

被引：33
|
作者：
Ji, Wenhua [1 ]
Xie, Hongkai [2 ]
Zhou, Jie [1 ,3 ]
Wang, Xiao [1 ,2 ]
Ma, Xiuli [2 ]
Huang, Luqi [3 ]
机构：
[1] Shandong Acad Sci, Shandong Anal & Test Ctr, Key Lab TCM Qual Control Technol, Jinan 250014, Peoples R China
[2] Shandong Agr Univ, Coll Food Sci & Engn, Tai An 270018, Shandong, Peoples R China
[3] China Acad Chinese Med Sci, Natl Resource Ctr Chinese Mat Med, State Key Lab Breeding Base Daodi Herbs, Beijing 100700, Peoples R China
来源：
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES | 2016年 / 1008卷
关键词：
Molecularly imprinted polymers; HPLC; Natural products; Dencichine; Panax notoginseng; DUMMY TEMPLATES; RECOGNITION; SEPARATION; SORBENT; REMOVAL; PLASMA; ACIDS;
D O I：
10.1016/j.jchromb.2015.11.053
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Specific molecularly imprinted polymers for dencichine were developed for the first time in this study by the bulk polymerization using phenylpyruvic acid and in-tyrosine as multi-templates. The photographs confirmed that molecularly imprinted polymers prepared using N,N'-methylene diacrylamide as crosslinker and glycol dimethyl ether as porogen displayed excellent hydrophilicity. Selectivity, adsorption isotherm and adsorption kinetics were investigated. The sample loading-washing-eluting solvent was optimized to evaluate the property of molecularly imprinted solid phase extract. Compared with LC/WCX-SPE, water-compatible molecularly imprinted solid phase extraction displayed more excellent specific adsorption performance. The extracted dencichine from Panax notoginseng with the purity of 98.5% and the average recovery of 85.6% (n = 3) was obtained. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：225 / 233
页数：9
相关论文
共 50 条
  • [41] Development of a Lower Toxic Approach Based on Green Synthesis of Water-Compatible Molecularly Imprinted Nanoparticles for the Extraction of Hydrochlorothiazide from Human Urine
    Arabi, Maryam
    Ghaedi, Mehrorang
    Ostovan, Abbas
    ACS SUSTAINABLE CHEMISTRY & ENGINEERING, 2017, 5 (05): : 3775 - 3785
  • [42] Molecularly Imprinted Polymers for Selective Extraction of Oblongifolin C from Garcinia yunnanensis Hu
    Wang, Liping
    Fu, Wenwei
    Shen, Yunhui
    Tan, Hongsheng
    Xu, Hongxi
    MOLECULES, 2017, 22 (04):
  • [43] Synthesis, characterization, and application of griseofulvin surface molecularly imprinted polymers as the selective solid phase extraction sorbent in rat plasma samples
    Bashir, Kamran
    Guo, Pengqi
    Chen, Guoning
    Li, Yunzhe
    Ge, Yanhui
    Shu, Hua
    Fu, Qiang
    ARABIAN JOURNAL OF CHEMISTRY, 2020, 13 (02) : 4082 - 4091
  • [44] Molecularly Imprinted Polymers-Curcuminoids and Its Application for Solid Phase Extraction
    Wulandari, Meyliana
    Amran, M. B.
    Lopez, A. B. Descalzo
    Urraca, J. L.
    Moreno-Bondi, M. C.
    4TH INTERNATIONAL CONFERENCE ON MATHEMATICS AND NATURAL SCIENCES (ICMNS 2012)L: SCIENCE FOR HEALTH, FOOD AND SUSTAINABLE ENERGY, 2014, 1589 : 400 - 403
  • [45] Molecularly imprinted polymers based on SBA-15 for selective solid-phase extraction of baicalein from plasma samples
    He, Hongliang
    Gu, Xiaoli
    Shi, Liying
    Hong, Junli
    Zhang, Hongjuan
    Gao, Yankun
    Du, Shuhu
    Chen, Lina
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2015, 407 (02) : 509 - 519
  • [46] Dummy Fragment Template Molecularly Imprinted Polymers for the Selective Solid-phase Extraction of Gonyautoxins from Seawater
    He, Xiuping
    Wang, Jiangtao
    Mei, Xiaoqi
    ANALYTICAL LETTERS, 2017, 50 (12) : 1877 - 1886
  • [47] Green synthesis of water-compatible layer-by-layer assembled sandwich bread-like molecularly imprinted polymers for selective recognition of baicalin from Scutellariae Radix
    Zhang, Yanhui
    Li, Hongbo
    Hai, Xiaoqin
    Lu, Qingxin
    Niu, Jiaxiao
    Fu, Ruiyu
    Guo, Xiaoli
    Di, Xin
    JOURNAL OF CHROMATOGRAPHY A, 2025, 1743
  • [48] Molecularly Imprinted Polymers for Selective Solid-Phase Extraction of Verapamil from Biological Fluids and Human Urine
    Javanbakht, Mehran
    Shaabani, Narges
    Abdouss, Majid
    Ganjali, Mohammad R.
    Mohammadi, Ali
    Norouzi, Parviz
    CURRENT PHARMACEUTICAL ANALYSIS, 2009, 5 (03) : 269 - 276
  • [49] Synthesis and application of a molecularly imprinted polymer in selective solid-phase extraction of efavirenz from water
    Mtolo, Sinothando P.
    Mahlambi, Precious N.
    Madikizela, Lawrence M.
    WATER SCIENCE AND TECHNOLOGY, 2019, 79 (02) : 356 - 365
  • [50] A molecularly imprinted polymer for the selective solid-phase extraction of dimethomorph from ginseng samples
    Xu, Xuanwei
    Liang, Shuang
    Meng, Xinxin
    Zhang, Min
    Chen, Ying
    Zhao, Dan
    Li, Yueru
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2015, 988 : 182 - 186
12345