NMR and conformational studies of new 5-phenylpyrrole-carboxamide derivatives

被引：2

作者：

Lopez-Cara, Luisa C. ^{[1
]}

Pineda de las Infantas, M. Jose ^{[1
]}

Carrion, M. Dora ^{[1
]}

Encarnacion Camacho, M. ^{[1
]}

Gallo, Miguel A. ^{[1
]}

Espinosa, Antonio ^{[1
]}

Entrena, Antonio ^{[1
]}

机构：

[1] Univ Granada, Fac Farm, Dept Quim Organ & Farmaceut, E-18071 Granada, Spain

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 2009年 / 47卷 / 12期

关键词：

NMR; H-1; C-13; HMQC; HMBC; NOEDIFF; 5-phenyl-1H-pyrrole-2-carboxamides;

D O I：

10.1002/mrc.2524

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The H-1 and C-13 NMR resonances of 22 5-(5-substituted-2-nitrophenyl)-1H-pyrrole-2-carboxamides, 22 5-(5-substituted-2-aminophenyl)-1H-pyrrole-2-carboxamides, and 9 5-phenyl-1H-pyrrole-2-carboxamides were assigned completely using the concerted application of one- and two-dimensional experiments (DEPT, gs-HMQC and gs-HMBC). NOE studies and conformational analysis confirm the preferred conformations of such compounds. Copyright (C) 2009 John Wiley & Sons, Ltd.

引用

页码：1101 / 1109

页数：9