Synthesis of nanocrystalline MoSe2 by sonochemical reaction of Se with Mo(CO)6

被引：20

作者：

Kristl, M ^{[1
]}

Drofenik, M ^{[1
]}

机构：

[1] Univ Maribor, Fac Chem & Chem Engn, SI-2000 Maribor, Slovenia

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2003年 / 6卷 / 01期

关键词：

sonochemical reaction; selenides; nanostructures;

D O I：

10.1016/S1387-7003(02)00685-8

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Nanocrystalline MoSe2 was prepared by a sonochemical reaction between Mo(CO)(6) and Se in decalin at 273 K in nitrogen atmosphere. The products were characterized by X-ray powder diffraction (XRD), transmission electron microscope (TEM), energy-dispersive X-ray spectroscopy (EDXS) and thermal analysis (TG and DSC). The XRD patterns showed that the product is amorphous, while annealing at 330degreesC yields nanocrystalline MoSe2. The influence of ultrasound and temperature is discussed. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：68 / 70

页数：3

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