Synthesis of the Ni-Zn-Sm ferrites using microwaves energy

被引:17
作者
Costa, A. C. F. M. [1 ]
Vieira, D. A. [1 ]
Silva, V. J. [1 ]
Diniz, V. C. S. [1 ]
Kiminami, R. H. G. A. [2 ]
Gama, L. [1 ]
机构
[1] Univ Fed Campina Grande, DEMa, BR-58109970 Campina Grande, PB, Brazil
[2] Univ Fed Sao Carlos, DEMa, BR-13565905 Sao Carlos, SP, Brazil
关键词
Ni-Zn-Sm ferrites; X-ray diffraction; Microwave energy;
D O I
10.1016/j.jallcom.2008.08.096
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
This work reports the preparation of Ni-Zn-Sm ferrite powders by combustion reaction using microwaves energy and XRD characterization. The influence of the fuel type used was investigated. The metallic nitrates and fuels (urea,glycine or 1:1 mixture) were heated in microwave oven for 5 and 10 min using the power of 450 and 630W. Ni-Zn-Sm ferrite and traces of secondary phases were observed in the powders obtained with glycine and mixture (1:1). The powers obtained with urea presented low cristallinity, only the main peak of the Ni-Zn-Sm ferrite phase was observed. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:37 / 39
页数:3
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