Crystal structure of the molecular inclusion complex of 5, 17-di-t-butyl-26, 28-disubstituted calix[4]arene with acetone (1:3)

被引：7

作者：

Lu, GY ^{[1
]}

Liu, F ^{[1
]}

Liu, YJ ^{[1
]}

He, WJ ^{[1
]}

Li, Q ^{[1
]}

Zhu, LG ^{[1
]}

机构：

[1] Nanjing Univ, State Key Lab Coordinat Chem, Dept Chem, Nanjing 210093, Peoples R China

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 1999年 / 29卷 / 10期

基金：

中国国家自然科学基金;

关键词：

calix[4]arene; acetone; inclusion complex;

D O I：

10.1023/A:1009514026129

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Crystal structure of inclusion complex of 5, 17-di-t-butyl-26, 28-disubstituted calix[4]arene 3 with acetone, [(C54H58N2O6 . CH3COCH3) . 2CH(3)COCH(3)], was determined by X-ray crystallographic analysis. It possesses space group C2/c, with a = 26.277(8), b = 12.967(5), c = 20.355(4) Angstrom, beta = 124.845(14)degrees, and D-calc = 1.173 mg/m(3) for Z = 4. Crystal data indicate that action of one molecule of compound 3 upon three molecules of acetone forms a clathrate intermolecular inclusion complex.

引用

页码：1121 / 1125

页数：5

共 4 条

[1] Crystal structure of the molecular inclusion complex of 5, 17-di-t-butyl-26, 28-disubstituted calix[4]arene with acetone (1:3)
Guoyuan Lu
Fang Liu
Yongjiang Liu
Weijiang He
Qian Li
Longgen Zhu
Journal of Chemical Crystallography, 1999, 29 : 1121 - 1125
[2] Crystal structure of the molecular inclusion complex tetra-p-nitro-tetra-O-butyl calix[4]arene with acetone (1:2)
Guoyuan Lu
Wei Song
Xiaobin Wan
Journal of Chemical Crystallography, 2000, 30 : 185 - 188
[3] Crystal structure of the molecular inclusion complex tetra-p-nitro-tetra-O-butyl calix[4]arene with acetone (1:2)
Lu, GY
Song, W
Wan, XB
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2000, 30 (03) : 185 - 188
[4] Studies on the inclusion property of 5,11,17,23-tetra-tert-butyl-25,26, 27,28-tetrakis[3-(methoxycarbonyl)benzyloxy]calix[4]arene
Zhou, ZX
Shi, YL
Du, CX
Xing, YJ
Wu, YJ
CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 2002, 23 (12): : 2281 - 2283

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