Preparation of monodispersed zinc sulfide microspheres by hydrothermal method

被引:0
作者
Wang Chang-Yan [1 ]
Yu Jian-Chang [1 ]
机构
[1] Fuzhou Univ, Coll Mat Sci & Engn, Fuzhou 350000, Peoples R China
关键词
zinc sulfide microspheres; surfactant P123; monodispersed; hydrothermal method;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Zinc sulfide microspheres are synthesized via a hydrothermal method, using surfactant P123 as template, and a possible mechanism of P123 as template for fabricating zinc sulfide microspheres was proposed. TEM, XRD, N-2 adsorption-desorption isotherms and FT-IR spectra were used for characterization. It shows that the zinc sulfide microspheres with diameter of 500 similar to 600 nm is comprised of ZnS nanocrystals with diameter of 6 similar to 7 mn. It is not only smooth and round, but also monodispersed. FT-IR spectra show that it is transparent from 4000 to 400 cm(-1). Therefore it is potential in many other fields such as optics, electronics, magnetics and so on.
引用
收藏
页码:2287 / 2290
页数:4
相关论文
共 16 条
[1]   POLY(ETHYLENE OXIDE)-POLY(PROPYLENE OXIDE)-POLY(ETHYLENE OXIDE) BLOCK-COPOLYMER SURFACTANTS IN AQUEOUS-SOLUTIONS AND AT INTERFACES - THERMODYNAMICS, STRUCTURE, DYNAMICS, AND MODELING [J].
ALEXANDRIDIS, P ;
HATTON, TA .
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 1995, 96 (1-2) :1-46
[2]  
AUTHONY JP, 1990, J POLYM SCI A, V28, P2485
[3]   OPTICAL-PROPERTIES OF MANGANESE-DOPED NANOCRYSTALS OF ZNS [J].
BHARGAVA, RN ;
GALLAGHER, D ;
HONG, X ;
NURMIKKO, A .
PHYSICAL REVIEW LETTERS, 1994, 72 (03) :416-419
[4]  
HUANG JM, 1996, J FUNCT POLYM, V9, P377
[5]   Theoretical study of the electronic structure of PbS nanoclusters [J].
Kane, RS ;
Cohen, RE ;
Silbey, R .
JOURNAL OF PHYSICAL CHEMISTRY, 1996, 100 (19) :7928-7932
[6]   Surface drug removal from ibuprofen-loaded PLA microspheres [J].
Leo, E ;
Forni, F ;
Bernabei, MT .
INTERNATIONAL JOURNAL OF PHARMACEUTICS, 2000, 196 (01) :1-9
[7]   Hydrothermal synthesis of novel sandwich-like structured ZnS/octylamine hybrid nanosheets [J].
Li, JP ;
Xu, Y ;
Wu, D ;
Sun, YH .
SOLID STATE COMMUNICATIONS, 2004, 130 (09) :619-622
[8]  
MA JP, 2005, J QIQIHAR U, V21, P5
[9]   Facile synthesis of hollow ZnS nanospheres in block copolymer solutions [J].
Ma, YR ;
Qi, LM ;
Ma, JM ;
Cheng, HM .
LANGMUIR, 2003, 19 (09) :4040-4042
[10]   SYNTHESIS AND CHARACTERIZATION OF NEARLY MONODISPERSE CDE (E = S, SE, TE) SEMICONDUCTOR NANOCRYSTALLITES [J].
MURRAY, CB ;
NORRIS, DJ ;
BAWENDI, MG .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (19) :8706-8715