Toroidal diamond anvil cell for detailed measurements under extreme static pressures

被引:130
作者
Dewaele, Agnes [1 ]
Loubeyre, Paul [1 ]
Occelli, Florent [1 ]
Marie, Olivier [1 ]
Mezouar, Mohamed [2 ]
机构
[1] CEA, DAM, DIF, F-91297 Arpajon, France
[2] ESRF, BP220, F-38043 Grenoble, France
来源
NATURE COMMUNICATIONS | 2018年 / 9卷
关键词
X-RAY-DIFFRACTION; EQUATION-OF-STATE; COMPRESSION; STRAIN; TEMPERATURE; ALUMINUM; HELIUM; METALS; ARGON; IRON;
D O I
10.1038/s41467-018-05294-2
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
Over the past 60 years, the diamond anvil cell (DAC) has been developed into a widespread high static pressure device. The adaptation of laboratory and synchrotron analytical techniques to DAC enables a detailed exploration in the 100 GPa range. The strain of the anvils under high load explains the 400 GPa limit of the conventional DAC. Here we show a toroidal shape for a diamond anvil tip that enables to extend the DAC use toward the terapascal pressure range. The toroidal-DAC keeps the assets for a complete, reproducible, and accurate characterization of materials, from solids to gases. Raman signal from the diamond anvil or X-ray signal from the rhenium gasket allow measurement of pressure. Here, the equations of state of gold, aluminum, and argon are measured with X-ray diffraction. The data are compared with recent measurements under similar conditions by two other approaches, the double-stage DAC and the dynamic ramp compression.
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页数:9
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