In situ neutron powder diffraction and structure determination in controlled humidities

被引：16

作者：

Ting, Valeska P. ^{[1
]}

Henry, Paul F. ^{[2
]}

Schmidtmann, Marc ^{[3
]}

Wilson, Chick C. ^{[3
]}

Weller, Mark T. ^{[1
]}

机构：

[1] Univ Southampton, Sch Chem, Southampton SO9 5NH, Hants, England

[2] Helmholtz Zentrum Berlin Mat & Energie, MI 1, Berlin, Germany

[3] Univ Glasgow, Dept Chem, WestCHEM, Glasgow G12 8QQ, Lanark, Scotland

来源：

CHEMICAL COMMUNICATIONS | 2009年 / 48期

基金：

英国工程与自然科学研究理事会;

关键词：

CRYSTAL-STRUCTURE; X-RAY; WATER;

D O I：

10.1039/b918702b

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A controlled-humidity sample environment has been constructed, allowing bulk powder samples undergoing humidity-induced phase transitions and reactions to be studied via in situ neutron diffraction. Associated developments in data collection and analysis permit this to be achieved without the use of D2O.

引用

页码：7527 / 7529

页数：3

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